Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified. Concept Introduction : Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Question

Want to see the full answer?

Answer 1

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Expert Solution & Answer

Want to see the full answer?

Check out a sample textbook solution

See solution

Students have asked these similar questions

5. You have 100 mL of a solution of benzoic acid in water; the amount of benzoic acid in the solution is estimated to be 0.30 g. The distribution coefficient of benzoic acid in diethyl ether and water is approximately 10. Calculate the amount of benzoic acid that would be left in the water solution after four 20-mL extractions with ether. Do the same calculation using one 80-mL extraction with ether to determine which method is more efficient. You must show all your work for this question (all calculations) to get any credit.

A mixture of the two compounds shown below is dissolved in ether. Using the information given in the experiment, select all the correct statements regarding the extraction and isolation of the two compounds. lose 0000 X OH A. X can be extracted from the organic layer using sodium hydroxide. B. Y can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of Y. C. X can precipitate out of the aqueous layer by the addition of sodium hydroxide to the salt of X. D. Y can be extracted from the organic layer using sodium hydroxide.

6. If more polar impurities are desired to be eluted first and then analyte, then at which stage do you need a strong organic solvent, such as methanol, when preparing samples with solid phase extraction A. Conditioning and loading b. Loading and eluting c. Washing and eluting d. Conditioning and washing e. Conditioning and eluting 7. If more polar impurities are desired to be eluted first and then analyte, then at which stage do you need a medium strength solvent, for example a mixture of methanol- water or methanol-buffer, when preparing samples with solid phase extraction A. Washing and loading b. eluting c. Conditioning d. Washing and eluting e. washing

Answer 2

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Expert Solution & Answer

Want to see the full answer?

Check out a sample textbook solution

See solution

Answer 3

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Expert Solution & Answer

Want to see the full answer?

Check out a sample textbook solution

See solution

Answer 4

Question

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Expert Solution & Answer

Want to see the full answer?

Check out a sample textbook solution

See solution

Answer 5

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 6

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 7

Chapter 6.3, Problem 15E

(a)

Interpretation Introduction

Interpretation:

Functional group present in 9-fluorenone (6) other than the aromatic rings should be identified.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 8

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 9

(b)

Interpretation Introduction

Interpretation:

More polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by a collection of eluted fractions.

Answer 10

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 11

(c)

Interpretation Introduction

Interpretation:

From fluorine and 9-fluorenone, first eluting compound that expects from a normal − phase column chromatography should be identified and the reason should be explained

Concept Introduction :

Column chromatography is a large scale solid-liquid adsorption chromatographic technique that can separate multi-gram amounts of mixtures. This is a preparative version of thin layer chromatography that permits separation and isolation of products by the collection of eluted fractions.

Answer 12

Expert Solution & Answer

Answer 13

Expert Solution & Answer

Answer 14

Want to see the full answer?

Check out a sample textbook solution

See solution

Answer 15

Ch. 6.2 - Prob. 1E Ch. 6.2 - Prob. 2E Ch. 6.2 - Prob. 3E Ch. 6.2 - Prob. 4E Ch. 6.2 - Prob. 5E Ch. 6.2 - Prob. 6E Ch. 6.2 - Prob. 7E Ch. 6.2 - Prob. 8E Ch. 6.2 - Prob. 9E Ch. 6.3 - Prob. 1E

Solution Summary: The author explains that polar compounds from fluorine and 9-fluorenone should be identified and explained.

Concept explainers

Videos

Want to see the full answer?

Chapter 6 Solutions