(a)
Interpretation:
The reason for the streak formation on silica gel TLC plates by carboxylic acids and addition of acetic acid to reduce the streaking should be explained.
Concept Introduction:
Thin Layer Chromatography is a sensitive chromatographic technique which used to analyze small quantities of the samples by solid-liquid adsorption method. Rectangular glass plate is coated with an adsorbent, sample to be analyzed is run on the plate in the developing chamber with the mobile phase to give spots of the analyzed sample.
(b)
Interpretation:
The chemical component which has to use to reduce the streaking on the TLC caused by the amine should be identified.
Concept Introduction:
Thin Layer Chromatography is a sensitive chromatographic technique which used to analyze small quantities of the samples by solid-liquid adsorption method. Rectangular glass plate is coated with a adsorbent, sample to be analyzed is run on the plate in the developing chamber with the mobile phase to give spots of the analyzed sample.
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Chapter 6 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
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- 1. _________________is used in the process of paper chromatography. A. Filter Paper B. Whatman Paper 2. In the dilution formula, N1V1=N2V2, N2 is ________. A. normality the concentrated solution B. normality of the desired solution 3. The reactivity of the alkaline earth metals in the decreasing order of __________. A. Be, Mg, Ca, Sr, B. Sr, Ca, Mg, Be 4. The chemical reaction of Br H20 + n-hexane produced __________. A. two layers of colorless solution B. orange and yellow layered solution C. violet and reddish brown layered solution 5. The _________ is used to transfer solid substances from container to another. A. Spatula B. Pippete C. Stirring rodarrow_forwardIt is not of the solute property detector used in HPLC is: a. Refractive index detector b. UV detector c. fluorescence detector d. UV-visible detectorarrow_forwardIn column chromatography, dyes with higher polarities tend to attach to which of the forbwing? A. THF-Acetone B. Silica C. Acetone D. Tetrahydrofuranarrow_forward
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