EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
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Chapter 3.3, Problem 24E

a)

Interpretation Introduction

Interpretation:Reason for streaks of carboxylic acid on silica gel TLC plates should be determined.

Concept introduction:TLC or thin layer chromatography is technique that is used to separate various components of mixture with help of stationary phase and mobile phase. It makes use of silica gel, cellulose or aluminum oxide. This procedure is widely used because of its simplicity, low cost efficiency, and high sensitivity.

b)

Interpretation Introduction

Interpretation:Purpose of addition of acetic acid to reduce streaking should be explained.

Concept introduction:TLC or thin layer chromatography is technique that is used to separate various components of mixture with help of stationary phase and mobile phase. It makes use of silica gel, cellulose or aluminum oxide. This procedure is widely used because of its simplicity, low cost efficiency, and high sensitivity.

c)

Interpretation Introduction

Interpretation:Substance that can be added to reduce streaks produced by amine on its TLC on silica gel should be determined.

Concept introduction:TLC or thin layer chromatography is technique that is used to separate various components of mixture with help of stationary phase and mobile phase. It makes use of silica gel, cellulose or aluminum oxide. This procedure is widely used because of its simplicity, low cost efficiency and high sensitivity.

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Which of the following statement is false?   a.   Component with the strong attraction to the support move more slowly than component with weak attraction.   b.   Chromatography technique used to separate only colored compounds.   c.   On TLC, single spot does not mean or guarantee a single substance (compound).   d.   Iodine vapor and UV- lamp are methods used for visualization uncolored compounds.
2. When separating acetone (an organic liquid) from LiBr (a solid impurity), which would be the most convenient means of separation? a. steam distillation b. column chromatography c. fractional distillation d. simple distillation Your answer:
What compounds present in a sample that can cause error in the analysis and alter desired results?   A. Matrix B. Selectivity C. Analyte D. Interference
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