EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
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Question
Chapter 3.2, Problem 27E
Interpretation Introduction
Interpretation:Purpose to scratch inside of flask with glass rod should be determined. Also, other methods to induce crystallization should be determined.
Concept introduction:Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
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Chapter 3 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
Ch. 3.2 - Prob. 1ECh. 3.2 - Prob. 2ECh. 3.2 - Prob. 3ECh. 3.2 - Prob. 4ECh. 3.2 - Prob. 5ECh. 3.2 - Prob. 6ECh. 3.2 - Prob. 7ECh. 3.2 - Prob. 8ECh. 3.2 - Prob. 9ECh. 3.2 - Prob. 10E
Ch. 3.2 - Prob. 11ECh. 3.2 - Prob. 12ECh. 3.2 - Prob. 13ECh. 3.2 - Prob. 14ECh. 3.2 - Prob. 15ECh. 3.2 - Prob. 16ECh. 3.2 - Prob. 17ECh. 3.2 - Prob. 18ECh. 3.2 - Prob. 19ECh. 3.2 - Prob. 20ECh. 3.2 - Prob. 21ECh. 3.2 - Prob. 22ECh. 3.2 - Prob. 23ECh. 3.2 - Prob. 24ECh. 3.2 - Prob. 25ECh. 3.2 - Prob. 26ECh. 3.2 - Prob. 27ECh. 3.2 - Prob. 28ECh. 3.2 - Prob. 29ECh. 3.2 - Prob. 30ECh. 3.2 - Prob. 31ECh. 3.2 - Prob. 32ECh. 3.2 - Prob. 34ECh. 3.3 - Prob. 1ECh. 3.3 - Prob. 2ECh. 3.3 - Prob. 3ECh. 3.3 - Prob. 4ECh. 3.3 - Prob. 5ECh. 3.3 - Prob. 6ECh. 3.3 - Prob. 7ECh. 3.3 - Prob. 8ECh. 3.3 - Prob. 10ECh. 3.3 - Prob. 11ECh. 3.3 - Prob. 12ECh. 3.3 - Prob. 13ECh. 3.3 - Prob. 14ECh. 3.3 - Prob. 15ECh. 3.3 - Prob. 16ECh. 3.3 - Prob. 17ECh. 3.3 - Prob. 18ECh. 3.3 - Prob. 19ECh. 3.3 - Prob. 21ECh. 3.3 - Prob. 22ECh. 3.3 - Prob. 23ECh. 3.3 - Prob. 24ECh. 3.3 - Prob. 25ECh. 3.3 - Prob. 26E
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- In fractional distillation, liquid can be seen running from the bottom of the distillation column back into the distilling flask. What effect does this returning condensate have on the fractional distillation?arrow_forwardGive a fundamental description of the recrystallization process. Explain why it is required and how it can be executed.arrow_forwardAn ideal solvent to use for recrystallization is one that: Group of answer choices dissolves the desired compound in ice-cold water temperature but does not dissolve the desired compound at its boiling temperature. a solvent in which the desired compound dissolves at any temperature. a solvent that reacts with the desired compound. dissolves the desired compound at its boiling temperature but does not dissolve the desired compound in ice-cold temperature.arrow_forward
- Just because there appears to be a good match between solubility characteristics between solute and solvent doesn’t mean you’ve found a good system. For example, benzyl alcohol appears to have favorable solubility characteristics with fluorenol, but it is a poor choice of solvent. Explain why this might be.arrow_forwardWhy is the freezing point of a pure solvent constant, while that a solution decrease with steady cooling?arrow_forwardIn the technique of recrystallization, one step involves heating the solvent containing the solute to its boiling point and, after the solution is cooled to room temperature, cooling it further in an ice-water bath. Why is it important to operate at these temperature extremes during a recrystallization?arrow_forward
- Fractional distillation of the 50:50 mixture of two miscible liquids gave the following distillation curve. What are their boiling points?arrow_forwardA chemist is given a nonelectrolyte white powder for analysis. 38.7 g of this substance is dissolved in 100.0 g of water. It is determined that the resulting solution freezes at -4.0°C. Additionally, the elemental composition of the substance is identified and found to be 40.0% C, 6.7% H and 53.3 % O by mass. Find the molecular formula of this unknown white powder using these experimental evidences (Kf of water: 1.86°C/m, C: 12 g/mol, H: 1 g/mol, O: 16 g/mol).arrow_forward
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