You have completed a synthesis and are now obtaining a melting point of the synthesized compound. The literature melting point is 126.2 °C - 128.4 °C. You determine the melting point to be 121.5 °C - 126.8 °C with a run at 2 °C per minute. You also determine that there is an erroneous signal in your IR spectrum. Which statement most accurately describes what you have going on here? O Your compound is not pure and is undergoing melting point depression. You may have added too much sample. None of these are correct. You may have added not enough sample. O There isn't an issue here, melting points are off all of the time.
Analyzing Infrared Spectra
The electromagnetic radiation or frequency is classified into radio-waves, micro-waves, infrared, visible, ultraviolet, X-rays and gamma rays. The infrared spectra emission refers to the portion between the visible and the microwave areas of electromagnetic spectrum. This spectral area is usually divided into three parts, near infrared (14,290 – 4000 cm-1), mid infrared (4000 – 400 cm-1), and far infrared (700 – 200 cm-1), respectively. The number set is the number of the wave (cm-1).
IR Spectrum Of Cyclohexanone
It is the analysis of the structure of cyclohexaone using IR data interpretation.
IR Spectrum Of Anisole
Interpretation of anisole using IR spectrum obtained from IR analysis.
IR Spectroscopy
Infrared (IR) or vibrational spectroscopy is a method used for analyzing the particle's vibratory transformations. This is one of the very popular spectroscopic approaches employed by inorganic as well as organic laboratories because it is helpful in evaluating and distinguishing the frameworks of the molecules. The infra-red spectroscopy process or procedure is carried out using a tool called an infrared spectrometer to obtain an infrared spectral (or spectrophotometer).
Trending now
This is a popular solution!
Step by step
Solved in 2 steps with 1 images
