Laboratory Techniques in Organic Chemistry
Laboratory Techniques in Organic Chemistry
4th Edition
ISBN: 9781464134227
Author: Jerry R. Mohrig, David Alberg, Gretchen Hofmeister, Paul F. Schatz, Christina Noring Hammond
Publisher: W. H. Freeman
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Chapter 14, Problem 2Q
Interpretation Introduction

Interpretation:

The reason for the observation of the range of melting point rather than an exact melting point should be determined.

Concept introduction:

The melting point of a crystalline substance is the temperature at which the substance starts changes into the liquid phase. Melting point is directly associated with the presence of intermolecular forces like hydrogen bonding, dipole-dipole interactions. High molecular symmetry, large surface area, polarity is associated with high melting points.

A pure compound melt at a narrow range and compounds with impurities have a wide range of melting points. Melting points are determined by filling the organic compound into the capillary tube with one end sealed.

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Laboratory Techniques in Organic Chemistry

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