Laboratory Techniques in Organic Chemistry
Laboratory Techniques in Organic Chemistry
4th Edition
ISBN: 9781464134227
Author: Jerry R. Mohrig, David Alberg, Gretchen Hofmeister, Paul F. Schatz, Christina Noring Hammond
Publisher: W. H. Freeman
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Chapter 10, Problem 3Q
Interpretation Introduction

Interpretation:

The precautions that are observed when sodium carbonate solution is used to extract an organic solution that contains acid traces should be determined.

Concept introduction:

A liquid-liquid extraction process uses two immiscible liquids for extraction. Immiscible liquids are insoluble in each other and form separate layers when placed in same glassware. It is a result of differences in polarities of the two liquids. The process of extraction is performed in a separating funnel.

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Write out the steps needed to separate hydrocarbon A and carboxylic acid B by using an extraction procedure.
What precautions should be observed when an aqueous sodium bicarbonate solution is used to extract and organic solution containing traces of acid? (Include a chemical equation)
1) To identify which contains more acid vinegar or lemon juice neutralization with sodium hydroxide can be used. Explain how. 2) The long filaments making up the thread of woven synthetic fabrics are likely polyesters. Describe the special characteristic that the alcohol and carboxylic acid must have so that they can react with each other to produce such long filaments.

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Laboratory Techniques in Organic Chemistry

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