In a two stage process acetic acid (A) is extracted from water (W) into hexanol (H) in a
liquid-liquid extraction vessel and the extract is subsequently separated by distillation.
Assume that water is completely insoluble in hexanol. A mixture of 18wt% acetic acid and
the balance water is fed to a liquid-liquid extraction vessel. Pure hexanol is fed to the
column to extract the acetic acid. The water-rich stream leaving the vessel is 99.5wt%
water and the balance acetic acid. The hexanol-rich extract from the vessel is fed to a
distillation column. The composition of the distillate is 96wt% acetic acid and the balance
hexanol. The bottoms stream contains 97.2wt% hexanol and recovers 95% of the hexanol
fed to the liquid-liquid extraction vessel.
a)Perform degrees of freedom analysis for overall system and subsystems.
b)Calculate the percentage of acetic acid in the process feed that is recovered in the
distillate stream.
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