Fundamentals Of Analytical Chemistry
9th Edition
ISBN: 9781285640686
Author: Skoog
Publisher: Cengage
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Based on the following 1H NMR spectra for LDA. Need help calculating the large and small coupling constants.

Transcribed Image Text:Batch 3
Sample 6
BRUKER
Current Data Parameters
NAME
EXPNO
PROCNO
3rdyr-210526
1
CH3
F2 - Acquisition Parameters
Date_
Time
20210526
12.08 h
„CH3
INSTRUM
spect
PROBHD
z104450_0319 (
CH3
zg30
65536
CDC13
16
2
8012.820 Hz
0.244532 Hz
4.0894465 sec
32
62.400 usec
17.77 usec
298.2 K
1.00000000 sec
1
400.1324708 MHz
PULPROG
TD
SOLVENT
NS
DS
HMS
FIDRES
AQ
RG
8.4
8.2
8.0
7.8
7.6
7.4
7.2
7.0
рpm
DW
DE
TE
D1
TDO
SFO1
NUC1
PO
P1
PLW1
1H
3.33 usec
10.00 usec
15.00000000 w
F2 - Processing parameters
65536
400.1300891 MHz
SI
SF
WDW
SB
EM
LB
0.30 Hz
GB
PC
1.00
8.
7
6
2
ppm
LO
96'0
0.87
00'L
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