Chemistry
Chemistry
10th Edition
ISBN: 9781305957404
Author: Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher: Cengage Learning
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Question

  1. Identify the solvent peak in the spectrum and list its chemical shift.

  2. Based on the chemical shifts, what functional groups are present in your compound? For

    each, correlate the functional group with the chemical shift of the identifying peak.

  3. List all the 13C NMR data in ACS journal style. The format is: 13C NMR (125 MHz,

    CDCl3): d list chemical shifts here.

Current Data Parameters NAME EXPNO PROCNO 1 F2 - Acquisition Parameters Date_ Time INSTRUM 20150706 9.46 spect 5 mm PABBO BB/ zgdc 187496 PROBHD PULPROG TD SOLVENT NS DS CDC13 31250.000 Hz 0.166670 Hz 2.9999361 sec 2050 16.000 usec 6.50 usec 295.9 K 2.00000000 sec 0.03000000 sec 1 SWH FIDRES AQ RG DW DE ТЕ D1 D11 TDO CHANNEL f1 =RE==-=== SFO1 NUC1 P1 125.7049802 MHz 130 10.00 usec 72.83999634 W PLW1 CHANNEL f2 499.8724993 MHz -E= ===R ==== =- SFO2 NUC2 CPDPRG [2 РСPD2 1H waltz16 80.00 usec 19.00000000 W 0.29688001 W PLW2 PLW12 TTTT 210 200 190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 ppm -205.018 - 40.818 =33.531 -15.215
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Transcribed Image Text:Current Data Parameters NAME EXPNO PROCNO 1 F2 - Acquisition Parameters Date_ Time INSTRUM 20150706 9.46 spect 5 mm PABBO BB/ zgdc 187496 PROBHD PULPROG TD SOLVENT NS DS CDC13 31250.000 Hz 0.166670 Hz 2.9999361 sec 2050 16.000 usec 6.50 usec 295.9 K 2.00000000 sec 0.03000000 sec 1 SWH FIDRES AQ RG DW DE ТЕ D1 D11 TDO CHANNEL f1 =RE==-=== SFO1 NUC1 P1 125.7049802 MHz 130 10.00 usec 72.83999634 W PLW1 CHANNEL f2 499.8724993 MHz -E= ===R ==== =- SFO2 NUC2 CPDPRG [2 РСPD2 1H waltz16 80.00 usec 19.00000000 W 0.29688001 W PLW2 PLW12 TTTT 210 200 190 180 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 ppm -205.018 - 40.818 =33.531 -15.215
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