Consider the following errors that could be made when running TLC. Indicate what should be done to correct the error.a. A two-component mixture containing 1-octene and 1,4-dimethylbenzene gave only one spot with an Rf value of 0.95. The solvent used was acetone.b. A two-component mixture containing a dicarboxylic acid and tricarboxylic acid gave only one spot with an Rf value of 0.05. The solvent used was hexane.c. When a TLC plate was developed, the solvent front ran off the top of the plate.

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter5: Chromatography
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Consider the following errors that could be made when running TLC. Indicate what should be done to correct the error.
a. A two-component mixture containing 1-octene and 1,4-dimethylbenzene gave only one spot with an Rf value of 0.95. The solvent used was acetone.
b. A two-component mixture containing a dicarboxylic acid and tricarboxylic acid gave only one spot with an Rf value of 0.05. The solvent used was hexane.
c. When a TLC plate was developed, the solvent front ran off the top of the plate.

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