Binary mixtures of NiO and Mo were prepared containing 20,50,and 80 weight percent of NiO. 20g of Al (internal standard) were added to 70 g of these mixtures and to 70 g of an unknown mixture of NiO and Mo. The intensity of suitable reflections were recorded. NiO(wt%)   Mo(wt%)  I(NiO)   I (Mo)   I (Al)   I(NiO)/I(Al)   I(Mo/IAl) 20                  80          73        639      246 50                  50         196       423      261 80                  20         508        271     423   Unknown                   227       364     263 Calculate I(NiO)/I(Al) and I(Mo)/I(Al) and plot vs % NiO and % Mo

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Binary mixtures of NiO and Mo were prepared containing 20,50,and 80 weight percent of NiO.

20g of Al (internal standard) were added to 70 g of these mixtures and to 70 g of an unknown mixture of NiO and Mo. The intensity of suitable reflections were recorded.

NiO(wt%)   Mo(wt%)  I(NiO)   I (Mo)   I (Al)   I(NiO)/I(Al)   I(Mo/IAl)

20                  80          73        639      246

50                  50         196       423      261

80                  20         508        271     423

  Unknown                   227       364     263

Calculate I(NiO)/I(Al) and I(Mo)/I(Al) and plot vs % NiO and % Mo respectively

Determine composition of unknown : wt % NiO and wt % Mo in unknown mixture

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