1. What is the retention time of molecule 9? 2. What happens to the peak area if the sample amount is doubled? 3. If run time is stopped at 5.5 mins, will molecules 8 & 6 be separated and quantified?

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.10QAP
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1. What is the retention time of molecule 9?
2. What happens to the peak area if the sample amount is doubled?
3. If run time is stopped at 5.5 mins, will molecules 8 & 6 be separated and quantified?
4. If the flow rate was doubled, will 8&6 be separated and quantified?
5. Does a single peak at time T in the chromatogram indicate only one compound is eluted?

0.799
0.699
0.599
0.499
0.399
0.299
0.199
0.099
-0.001
1.5
HN
Ph-
NH
Ph
7
Ph
Ph-
NH₂
29
Ph
3.5
-NH
2
Ph
Ph
OH
8
Ph
Ph-
5.5
Ph
6
time/min
1
Ph Ph
↓
Ми
PhPh 3
".
↓
ܝܝܝܐ
7.5
9.5
Transcribed Image Text:0.799 0.699 0.599 0.499 0.399 0.299 0.199 0.099 -0.001 1.5 HN Ph- NH Ph 7 Ph Ph- NH₂ 29 Ph 3.5 -NH 2 Ph Ph OH 8 Ph Ph- 5.5 Ph 6 time/min 1 Ph Ph ↓ Ми PhPh 3 ". ↓ ܝܝܝܐ 7.5 9.5
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