Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
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Chapter 33, Problem 33.7QAP
Sketch a flow injection apparatus for the determination of sodium sulfite in aqueous samples.
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What are desirable properties of a gravimetric precipitate?
Explain how a Gravimetric Analysis is performed.
Which among these is/are properties for the type of precipitate required in gravimetric analysis?
Hygroscopic
Known composition
Reactive with atmospheric constituents
Large particles
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- Why a precipitate of manganese dioxide be removed from the potassium permaganate solution before standardization?arrow_forward1. Differentiate the Faians method from the Volhard method of precipitation titrimetry, Include key information such as indicator used, endpoint, analytes, and the chemical reactions.arrow_forwardWhy are many ionic precipitates washed with electrolyte solution instead of pure water?arrow_forward
- A chemist received different mixtures for analysis with the statement that they contained NAOH, NaHCO3, Na,CO3 or compatible mixtures of these substances together with inert material. From the data given, identify the respective materials. Sample 4. The sample was titrated with acid until the pink of phenolphthalein disappeared; this process required 39.96 mL. On adding an excess of the acid, boiling and titrating back with NAOH, it was found that the base was equivalent to the excess acid. O A NazCO3, NaHCO3 OB. NaHCO3 O C. Na2CO3 O D. None of these O E. NaOHarrow_forwardA K2SO4 solution is prepared by weighing out a certain amount of the pure solid reagent,dissolving it to 500.0 mL in a volumetric flask. An aliquot was taken from this solution.of 25.00 ml and diluted to 500.0 ml. An aliquot of 5.00 was taken from this new solution anddiluted to 50.00 ml. A chemical analysis of this new solution showed a 0.100%(w/v)in K+. Calculate the weight of the pure solid K2SO4 used for the preparation of the original solution.and its concentration in each volumetric flask. The answer is 2.23x10^2garrow_forward16) Which of the following(s) is/are correct? I- Selectivity factor is the amount of time a solute spends in the stationary phase relative to the time it spends in mobile phase II- The retention time for an analyte is the time interval between its injection onto a column and its appearance at the detector at the other end of the column. III- Distribution constant is the ratio of the total solute concentration in the stationary phase to that in the mobile phase. A) I, II and III B) Only II C) I and III D) II and III E) Only III for GC2arrow_forward
- 6. In gravimetric analysis, an ideal precipitating agent should i) React specifically or at least selectively with the analyte. ii) React rapidly with the analyte. iii) React completely with the analyte iv) All the above.arrow_forward2.) A 0.2185g sample of NaCl was assayed using Volhard Method with 50mL 0f 0.0998N AgNO3 and 11.9mL of 0.1350N NH4SCN. Calculate the % NaCl in the sample.arrow_forwardWhich of the following statements is true? A Liquids can be weighed using a weighing paper. B In weighing hygroscopic substances, containers should always be kept close when not in use. After drying a sample in the oven, you can place it immediately inside the analytical balance. D Place solid reagents / precipitates directly on top of the balance pan.arrow_forward
- 1. (a) What are the requirements that should be met for a precipitation reaction to serve as the basis of a gravimetric method? (b) What is "digestion"? In what ways can digestion improve the quality of an analytical precipitate? (c) A typical thermogravimetric curve for magnesium oxalate (MgC:O.) precipitates is given below. 18 134 226 398 478 900 Temperature, C Describe the weight loss as a function of temperature. Select a suitable ignition temperature for the gravimetric analysis of magnesium. Explain your choice. i. Predict the possible composition of the residues collected at the chosen temperature, i.arrow_forwardQ1)a) In the gravimetric analysis the precipitate should be free from impurities. Give the detailed justification for the above statement by identifying impurities. b) It is required to analyse the metal from its ore sample. Manganese (Mn)present in the ore sample was analysed by forming a precipitate of MnSO4. If 2.98 g of ore sample gives 0.19 g of MnSO4. Calculate the percentage of Mn present in the sample.arrow_forwardMatching Type Arrange the following steps in the standardization of 0.1N AgNO3 * Carefully bring the mixture to a boil for approximately 5 minutes, then it stand in the dark for let however long it takes for the precipitate to settle and the liquid in the supernatant to clarify. Drying the precipitate to a constant weight at 110 °C. Pipette approximately 40 ml of the prepared silver nitrate solution, then add water to make approximately 100 ml. Using the dried constant weight of the silver chloride precipitate, determine the normality of the silver nitrate solution. The precipitate should be transferred to a tared filtering crucible and washed with small amounts of water that has been slightly acidified with nitric acid. Until the silver chloride has completely precipitated, heat the solution and gradually add diluted hydrochloric acid while stirring continuously. Step 1 O O Step 2 O O O Step 3 Step 4 Step 5 o o O O O O O O O Step 6 O O O O ο ο οarrow_forward
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