Problem 11 IR Spectrum (KBr disc) 1693 4000 3000 2000 1600 1200 800 V (cm) 10아 Mass Spectrum 56 M*- 112 80 No significant UV 60 absorption above 220 nm 200 240 280 40 80 120 m/e 160 13C NMR Spectrum % of base peak

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.16QAP
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Focus on the third and 4th spectra. Draw and label the peaks of each spectra. Give atleast 2 sentences to support your answer
Problem 11
IR Spectrum
(KBr disc)
1693
4000
3000
2000
1600
1200
800
V (cm" )
100-
56
Mass Spectrum
M*- 112
80
No significant UV
60
absorption above 220 nm
40
20
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(100.0 MHz, CDCI, solution)
DEPT CH CH CH
proton decoupled
solvent
200
160
120
80
40
0 8 (ppm)
1H NMR Spectrum
(400 MHz, CDCI, solution)
TMS
1
8 (ppm)
10
8
7
6.
3
2
% of base peak
Transcribed Image Text:Problem 11 IR Spectrum (KBr disc) 1693 4000 3000 2000 1600 1200 800 V (cm" ) 100- 56 Mass Spectrum M*- 112 80 No significant UV 60 absorption above 220 nm 40 20 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100.0 MHz, CDCI, solution) DEPT CH CH CH proton decoupled solvent 200 160 120 80 40 0 8 (ppm) 1H NMR Spectrum (400 MHz, CDCI, solution) TMS 1 8 (ppm) 10 8 7 6. 3 2 % of base peak
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