Instruction: (a) Based on the information provided, determine the structures of compounds. (b) Assign all peaks in ¹H and ¹³C NMR spectra of compounds Compound 5: 4000 delalalalalalalalal 100 80 60 IR Spectrum (liquid film) % of base peak 10 40 DEPT 13C NMR Spectrum (50.0 MHz, CDCI, solution) 3000 proton decoupled 200 ¹H NMR Spectrum (200 MHz, COCI, solution) 4.0 9 M+= 89 (<1%) 80 120 160 m/e expansion 2000 3.0 8 v (cm¹) 160 1553 7 2.0 1600 6 200 1387 120 1200 1.0 ppm Mass Spectrum 800 240 280 5 C₂H₂ NO₂ solvent 80 4 0.0 0.5 1.0 1.5 3 absorbance 200 40 UV spectrum 137.0 mg/10 mis path length: 0.2 cm solvent: ethanol 250 λ (nm) f 2 300 0 1 350 8 (ppm) TMS 0 8 (ppm)

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Instruction:
(a) Based on the information provided, determine the structures of compounds.
(b) Assign all peaks in ¹H and 2³C NMR spectra of compounds
Compound 5:
4000
100
delalalalalalalalal
IR Spectrum
(liquid film)
80
60
% of base peak
10
40
DEPT
13C NMR Spectrum
(50.0 MHz, CDCI, solution)
3000
proton decoupled
200
¹H NMR Spectrum
(200 MHz, CDCI, solution)
4.0
9
80
M+¹ = 89 (<1%)
expansion
3.0
2000
8
V (cm¹)
120 160
m/e
160
1553
7
2.0
1600
6
200
1387
120
1200
1.0 ppm
Mass Spectrum
800
240 280
5
C₂H₂ NO₂
solvent
80
4
0.0
0.5
1.0
1.5
3
absorbance
200
40
UV spectrum
137.0 mg/10 mis
path length: 0.2 cm
solvent: ethanol
250
λ (nm)
f
2
300
0
1
350
8 (ppm)
TMS
0
8 (ppm)
Transcribed Image Text:Instruction: (a) Based on the information provided, determine the structures of compounds. (b) Assign all peaks in ¹H and 2³C NMR spectra of compounds Compound 5: 4000 100 delalalalalalalalal IR Spectrum (liquid film) 80 60 % of base peak 10 40 DEPT 13C NMR Spectrum (50.0 MHz, CDCI, solution) 3000 proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) 4.0 9 80 M+¹ = 89 (<1%) expansion 3.0 2000 8 V (cm¹) 120 160 m/e 160 1553 7 2.0 1600 6 200 1387 120 1200 1.0 ppm Mass Spectrum 800 240 280 5 C₂H₂ NO₂ solvent 80 4 0.0 0.5 1.0 1.5 3 absorbance 200 40 UV spectrum 137.0 mg/10 mis path length: 0.2 cm solvent: ethanol 250 λ (nm) f 2 300 0 1 350 8 (ppm) TMS 0 8 (ppm)
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