Fully interpret and compare the 13C NMR spectrum and the 1H NMR spectrum of the compound (R,R)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine. Label and explain the peaks and why they show up where they do.

World of Chemistry, 3rd edition
3rd Edition
ISBN:9781133109655
Author:Steven S. Zumdahl, Susan L. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan L. Zumdahl, Donald J. DeCoste
Chapter13: Gases
Section: Chapter Questions
Problem 49A
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Fully interpret and compare the 13C NMR spectrum and the 1H NMR spectrum of the compound (R,R)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine. Label and explain the peaks and why they show up where they do. 

But
14
12
ОН НО
Bu
10
6
But
4
0.50
8
0.48
0.76
6
tBu
3.74
2
0.50573 5.10.26
73 37381 0.34
OpenVnmr
0
ppm
Transcribed Image Text:But 14 12 ОН НО Bu 10 6 But 4 0.50 8 0.48 0.76 6 tBu 3.74 2 0.50573 5.10.26 73 37381 0.34 OpenVnmr 0 ppm
CARBON 01
SOR_3rd_yr_C13
18d
170
-165.81
-157.99
160
150
139.87
-136.33
140
126.72
126.03
130
-117.85
120
110
100
90
77.33
+77.02
-76.70
-72.43
80
70
60
55
34.95
34.03
33.28
31.43
29.45
-24.37
30
-450
-350
-300
-250
150
-100
ọ
Transcribed Image Text:CARBON 01 SOR_3rd_yr_C13 18d 170 -165.81 -157.99 160 150 139.87 -136.33 140 126.72 126.03 130 -117.85 120 110 100 90 77.33 +77.02 -76.70 -72.43 80 70 60 55 34.95 34.03 33.28 31.43 29.45 -24.37 30 -450 -350 -300 -250 150 -100 ọ
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