EXPERIMENTAL RXN:- Mechanism - A (2 Preparation of Nickel Thiocyanate Solution :- When Ni(NO2),. 6H2O is dissolved in n-butanol: 2+ Ni(NO3)2 6H20 n-butanol, Ni² + + 2 NO₂ + 6H₂O. Then (heat) - Add Potassium thiocyanate (KSCN) to hot Ni (NO3)2 6H20 Solution, then it will produce Nickle thiocyanate in Solution & Precipitation of Potassium Nitrate (KNO3) Rx":- N2+ +2NCS → Ni(SCN)2 2KN03 (ppt) 2K+ + 2N03 Live To Prepare Triphenylphosphine in Sol?:- When Triphenylphosphine (PPh3) is dissolved in n-butanol by heating. Rxn- PPh 3 (s) n-butanol, PPh3 (Solution). liii formation of Dithiocyanatobis (triphenyl phosphine) Liis Nickel (11) (Ni(NCS), (PPh3)2} signdor M Add hot triphenylphosphine Solution to hot Nickel throcyanate Solution: (i) RxNi-wil 21 Octafsil 21° * Ni(NCS) +2PPh3 (Solution) [Ni(NCS), (PPho)] Tonstud-r Overall RXN: लता 11 stranussid muizenty bb Ni (NO3)2.6H₂O + 2 KNCS +2PPh31 >[Ni(SCN)2 (PPh3)2] + 2KN03+6H20 42214 2016
EXPERIMENTAL RXN:- Mechanism - A (2 Preparation of Nickel Thiocyanate Solution :- When Ni(NO2),. 6H2O is dissolved in n-butanol: 2+ Ni(NO3)2 6H20 n-butanol, Ni² + + 2 NO₂ + 6H₂O. Then (heat) - Add Potassium thiocyanate (KSCN) to hot Ni (NO3)2 6H20 Solution, then it will produce Nickle thiocyanate in Solution & Precipitation of Potassium Nitrate (KNO3) Rx":- N2+ +2NCS → Ni(SCN)2 2KN03 (ppt) 2K+ + 2N03 Live To Prepare Triphenylphosphine in Sol?:- When Triphenylphosphine (PPh3) is dissolved in n-butanol by heating. Rxn- PPh 3 (s) n-butanol, PPh3 (Solution). liii formation of Dithiocyanatobis (triphenyl phosphine) Liis Nickel (11) (Ni(NCS), (PPh3)2} signdor M Add hot triphenylphosphine Solution to hot Nickel throcyanate Solution: (i) RxNi-wil 21 Octafsil 21° * Ni(NCS) +2PPh3 (Solution) [Ni(NCS), (PPho)] Tonstud-r Overall RXN: लता 11 stranussid muizenty bb Ni (NO3)2.6H₂O + 2 KNCS +2PPh31 >[Ni(SCN)2 (PPh3)2] + 2KN03+6H20 42214 2016
Chapter1: Taking Risks And Making Profits Within The Dynamic Business Environment
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