Outline the experimental procedure including the mass and moles of the exact number of starting materials and productHow was the experiment conducted? what was the observations made during the reaction ProcedureDissolve 4.0 g of KOH pellets (cannot use NaOH) in 8 mL of water in a 250-mL round bottomflask (use the flask that contains two ground-glass openings (one for the condenser unit and theother for the separatory funnel). Add 2.0 grams of p-cresol to the round bottom flask in the hood.Swirl the mixture until the solution is homogeneous. Add three boiling stones. Fit the flask with areflux condenser and heat to a gentle boil. After the mixture has started to boil, add 6 mL of a50% aqueous solution (g/mL) of chloroacetic acid dropwise using a separatory funnel placed inthe side-arm of your round-bottom flask. After the addition of the chloroacetic acid solution,continue refluxing for another 10 minutes.After reflux, transfer the solution to a small beaker while it is still hot (if you let the mixture cool,solid forms inside the flask and it is more difficult to remove). You can overcome this problem byadding about 10 mL of water to the reaction mixture, and then pour this slightly diluted mixtureinto a 100-mL beaker. After you have poured the (diluted) reaction into the 100-mL beaker, let itcool to room temperature in the beaker. Acidify the solution with drop-wise addition ofconcentrated 12 M HCl. (Monitor the pH with pH/litmus paper to be certain pH is acidic, pH=2).It might be beneficial to ensure you do not isolate the potassium salt to heat the acidified mixturewith solids until it all dissolves at a higher temperature. Then, simply cool that mixture in an icebath to attain the maximal yield of a solid product. Be sure the precipitate has formed completely,perhaps storing it on ice for about 15 min before filtering it. Filter and collect the precipitatedproduct by using a Büchner funnel vacuum filtration setup. To the collected solid product from theprevious step, you will perform a re-crystallization step by adding the entire crude product toboiling water. Do not use more than 50 mL of water to ensure you will be able to isolate crystallineproducts. Collect your re-crystallized product using vacuum filtration. Allow the solid to dry untilthe next lab period in the designated drying oven.Weigh the solid to determine the yield. Also, determine the melting point after you havedetermined your yield for recovery of your product. Acquire the 'H and the 1C-NMR spectrum(in DMSO-d6).

The objective of this experiment should include the background of the reaction and the purpose of…

Dissolve 4.0 g of KOH pellets (cannot use NaOH) in 8 mL of water in a 250-mL round bo flask (use the flask that contains two ground-glass openings (one for the condenser unit an other for the separatory funnel). Add 2.0 grams of p-cresol to the round bottom flask in the Swirl the mixture until the solution is homogeneous. Add three boiling stones. Fit the flask v reflux condenser and heat to a gentle boil. After the mixture has started to boil, add 6 mL 50% aqueous solution (g/mL) of chloroacetic acid dropwise using a separatory funnel plac the side-arm of your round-bottom flask. After the addition of the chloroacetic acid solu tinuo roflu for another 10 minutos

Dissolve 4.0 g of KOH pellets (cannot use NaOH) in 8 mL of water in a 250-mL round bo flask (use the flask that contains two ground-glass openings (one for the condenser unit an other for the separatory funnel). Add 2.0 grams of p-cresol to the round bottom flask in the Swirl the mixture until the solution is homogeneous. Add three boiling stones. Fit the flask v reflux condenser and heat to a gentle boil. After the mixture has started to boil, add 6 mL 50% aqueous solution (g/mL) of chloroacetic acid dropwise using a separatory funnel plac the side-arm of your round-bottom flask. After the addition of the chloroacetic acid solu tinuo roflu for another 10 minutos

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter83: Simple Distillation

Section: Chapter Questions

Problem 2P

See similar textbooks

Similar questions

heating a mixture to 100 degrees is necessary to seperate a mixture only containing salt and sand true or false?
After water and benzene are mixed, we see two layers. A) True False B
Organic liquids are usually less dense than water. True False
Put some crushed ice in the 400 mL beaker. Allow some of the ice to melt then take the temperature. Record this as temperature of the ice. Temperature reading is 0.00°C Prepare accurately 20 % urea solution (2 grams urea in 8 grams distilled water). Place this solution in a hard glass test tube then place it in the beaker with crushed ice. Get the temperature of the urea solution at interval of 30 seconds. The temperature will go down until the freezing point is reached. Continue getting the temperature until 3 consecutive readings are identical. Record this as the freezing point of the solution. Temperature reading is -8.00°C. Make a general statement on the effect of solids upon the freezing point of liquid in which they are dissolved.
Weigh out accurately 9.99 g of copper(II) sulfate pentahydrate (CuSO4·5H2O) by taring using a clean and dry empty 250-ml beaker. 2. Add tap water to the beaker to reach the 50-mL mark on the side of the beaker. 3. Dissolve all the crystals of CuSO4·5H2O in the water using a clean glass rod for stirring. 4. Then using a glass funnel transfer all the blue solution to a 100-mL volumetric flask. Rinse the beaker with about 10 mL of water and transfer the solution to the volumetric flask. Repeat the rinsing of the beaker with another 10 mL of water and transfer the solution to the volumetric flask. This is called quantitative transfer of the solution. 5. Then add enough water to reach the calibration mark of the volumetric flask. (You will need to use a dropper to add the last few drops of water to ensure the meniscus is on the calibration mark). Close the volumetric flask with a stopper and mix the solution well (so that it is homogeneous). 6. You have now prepared a standard solution (or…
Filtration of samples A, B, and C show no residue left. After letting them dry in different beakers, SAmple A remains no residues. Sample B shows crystal leftovers, and sample C show brown film on the beaker walls. This means that: a. Two or more samples are heterogenous b. Two or more samples are homogenous c. all sample have 2 or more phases d. all samples are pure
If you are requested to compound 60 mL of the Concentrated Peppermint Water from the original amount of 500 mL of Concentrated Peppermint water containing: 10 mL of Peppermint Oil, 25 g talc, and 300 mL of 90% ethyl alcohol Calculate the volume of Peppermint Oil, required for the preparation. a 1.68 mL b 1.20 mL c 2.14 mL d 2.35 mL
The 50:50 (by mass) mix of water and ethylene glycol (antifreeze) contains 16 moles of ethylene glycol per 1 kg of water. Given than K₁ for water is 0.5 °C/m, what is the boiling point of the mixture? 100.5°C 108 °C 92°C 100°C 99.5°C
Which among the following is best used in separating heterogeneous mixtures of solids from liquids? O Mesh Strainers O Distillation Set-up O Filtration Set-up O Drying Oven
A 20ml mixture contains 10% volume methanol and 90% volume water. Find the mole fraction of water and methanol
Part E Write balanced complete ionic equation for NaOH(aq)+ HC,H,O2 (aq)→H,O(1) + NaC, H,O2 (aq). Express your answer as a chemical equation. Identify all of the phases in your answer. ΑΣΦ x" O That's not quite right. Please check your formatting and try again No credit lost. Try again. Submit Previous Answers Request Answer Part F Write balanced net ionic equation for NAOH(aq) | HC,H,O, (aq) H,O(1) i NaC, H,O, (aq). Express your answer as a chemical equation. Identify all of the phases in your answer.
What type of solid-liquid extraction is done when the tea leaves is boiled in water?