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Calculate the number of moles of aniline and 2,5-hexanedione to be used in synthesis of 2,5 dimethyl-1-phenylpyrrole
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- Several diamines are building blocks for the synthesis of pharmaceuticals and agro-chemicals. Show how both 1,3-propanediamine and 1,4-butanediamine can be prepared from acrylonitrile.Draw structural formulas for (1) the alkyltriphenylphosphonium salt formed by treatment of each haloalkane with triphenylphosphine, (2) the phosphonium ylide formed by treatment of each phosphonium salt with butyllithium, and (3) the alkene formed by treatment of each phosphonium ylide with acetone.Explain the experimental procedure of the laboratory preparation of the synthesis of benzyl chloride from phenol Explain the chemistry behind the synthesis of benzyl chloride from phenol
- Describe two synthetic routes for the preparation of p-methoxyaniline from benzene.What reactions and reagents can be used to make phenol from benzene if electrophilic aromatic substitution reactions are excluded and benzene is the only source of carbon?Synthetize 3-phenyl-2-propenoic acid from benzaldehyde using whatever organic/inorganic reagents are needed. 3-phenyl-2-propenoic = 3-phenylacrylic acid
- In preparation of dibenzalacetone from benzaldehyde: Give two techniques that can be used to purify partially air-oxidized benzaldehyde. Indicate how each technique works in purifying benzaldebyde from its air-oxidized impurities.Explain the experimental procedure of the laboratory preparation of the synthesis of Aniline from benzoic acid. Explain the chemistry behind the synthesis of Aniline from benzoic acid.What is the structure of the compound formed when 5-nitro-2-furaldehyde reacts with 4-cyanophenyl hydrazine hydrochloride?
- Propose a method to separate a mixture containing phenol, benzoic acid, naphthalene, and p-nitroaniline. Phenol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. Benzoic acid is soluble in either sodium hydroxide or sodium bicarbonate solutions. Write out the structures of the molecules in your scheme.Describe how 3-methyl-1-phenyl-3-pentanol can be prepared from benzene. You can use any inorganic reagents and solvents, and any organic reagents provided they contain no more than two carbons.Maletic anhydride 1,4-dimethoxybenzene benzil anthracene benzaldehyde benzoic acid 3-nitrophthalic acid salicylic acid benzophenone