4000 100 80 60 IR Spectrum (liquid film) 40 20 % of base peak expansion 40 13C NMR Spectrum (100.0 MHz, CDCI, solution) 7.5 10 3000 1H NMR Spectrum (400 MHz, CDCI, solution) proton decoupled 200 80 DEPT CH₂ CH₂ CH 7.3 ppm 1 9 1 8 2000 105 . 120 160 m/e TY m v (cm¹) M=134 160 7 1600 200 6 120 1200 2.8 2.7 ppm Mass Spectrum 800 240 280 1 5 C10H14 1 solvent 1 80 expansions 1.8 1.7 ppm 4 J UV Spectrum max 260 nm (log₁0€ 2.5) 40 1.45 1.35 ppm 3 I 2 0 1 8 (ppm) expansion 1.05 0.95 TMS 1 0 8 (ppm)
4000 100 80 60 IR Spectrum (liquid film) 40 20 % of base peak expansion 40 13C NMR Spectrum (100.0 MHz, CDCI, solution) 7.5 10 3000 1H NMR Spectrum (400 MHz, CDCI, solution) proton decoupled 200 80 DEPT CH₂ CH₂ CH 7.3 ppm 1 9 1 8 2000 105 . 120 160 m/e TY m v (cm¹) M=134 160 7 1600 200 6 120 1200 2.8 2.7 ppm Mass Spectrum 800 240 280 1 5 C10H14 1 solvent 1 80 expansions 1.8 1.7 ppm 4 J UV Spectrum max 260 nm (log₁0€ 2.5) 40 1.45 1.35 ppm 3 I 2 0 1 8 (ppm) expansion 1.05 0.95 TMS 1 0 8 (ppm)
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
Determine the structure of the compound using the information provided below, show the proton integration and the mass spectrometry fragments (ensure curly arrow mechanism).
Transcribed Image Text:4000
100
80
60
IR Spectrum
(liquid film)
20
wwwladdade
% of base peak
expansion
13C NMR Spectrum
(100.0 MHz, CDCI, solution)
7.5
10
3000
40
1H NMR Spectrum
(400 MHz, CDCI, solution)
80
proton decoupled
200
9
DEPT CH₂ CH₂ CH4
7.3 ppm
1
8
105
2000
120
.
mmp
V (cm¹)
M+= 134
m/e
160
1600
160
7
6
1200
120
2.8 2.7 ppm
Mass Spectrum
200 240 280
800
5
C10H14
1.8
solvent
80
expansions
4
UV Spectrum
max 260 nm (log₁08 2.5)
40
1.7 ppm 1.45 1.35 ppm
3
0
AHA
1.05 0.95
2
8 (ppm)
1
expansion
TMS
1
0
8 (ppm)
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