4000 100 80 60 IR Spectrum (liquid film) 40 20 % of base peak expansion 40 13C NMR Spectrum (100.0 MHz, CDCI, solution) 7.5 10 3000 1H NMR Spectrum (400 MHz, CDCI, solution) proton decoupled 200 80 DEPT CH₂ CH₂ CH 7.3 ppm 1 9 1 8 2000 105 . 120 160 m/e TY m v (cm¹) M=134 160 7 1600 200 6 120 1200 2.8 2.7 ppm Mass Spectrum 800 240 280 1 5 C10H14 1 solvent 1 80 expansions 1.8 1.7 ppm 4 J UV Spectrum max 260 nm (log₁0€ 2.5) 40 1.45 1.35 ppm 3 I 2 0 1 8 (ppm) expansion 1.05 0.95 TMS 1 0 8 (ppm)
4000 100 80 60 IR Spectrum (liquid film) 40 20 % of base peak expansion 40 13C NMR Spectrum (100.0 MHz, CDCI, solution) 7.5 10 3000 1H NMR Spectrum (400 MHz, CDCI, solution) proton decoupled 200 80 DEPT CH₂ CH₂ CH 7.3 ppm 1 9 1 8 2000 105 . 120 160 m/e TY m v (cm¹) M=134 160 7 1600 200 6 120 1200 2.8 2.7 ppm Mass Spectrum 800 240 280 1 5 C10H14 1 solvent 1 80 expansions 1.8 1.7 ppm 4 J UV Spectrum max 260 nm (log₁0€ 2.5) 40 1.45 1.35 ppm 3 I 2 0 1 8 (ppm) expansion 1.05 0.95 TMS 1 0 8 (ppm)
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.8QAP
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Determine the structure of the compound using the information provided below, show the proton integration and the mass spectrometry fragments (ensure curly arrow mechanism).
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