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- 7. A Cu2* solution obtained by dissolving a 3.1871-g penny in 500 mL of nitric acid has an absorbance of 0.342 at 620 nm in a 1.00 cm cell. The calibration curve prepared from Cu2+ solutions of varying concentrations has a slope of 281.8 L/mol and a y-intercept of 0.0106. (a) Calculate the concentration of the solution in moles per liter. (b) Calculate the percent Cu by mass in the penny5. (1) (ii) Ibuprofen (206.3 g/mol) absorbs at 255 nm and shows a molar absorptivity of 3010 L/mol.cm. A tablet of ibuprofen, 0.6654 g, was ground and 0.2203 g powder was dissolved in 20% methanol in a 100 mL volumetric flask (Solution A). Exactly 5.0 mL of Solution A was diluted in a 50.0 mL flask and the resulting solution showed an absorbance of 0.1228 AU in a 1.00 cm cell. (i) What is the concentration (mol/L) of ibuprofen in the 100 mL stock solution? (ii) Report the amount of ibuprofen in mg/Tablet. Ibuprofen H3C | HCCH; 1 H3C CH3 -CH-COOH(a) Describe step-by-step procedure how you would use atomic absorption to measure copper in urine?
- A chemist obtained the following data for percent lindane in the triplicate analysis of an insecticide preparation: 7.23, 6.95, and 7.53%. Calculate the 90% confidence interval for the mean of the the three data, assuming that (a) the only information about the precision of the method is the precision for the three data. (b) on the basis of long experience with the method, it is believed that s---->σ lindane. (c) If s=0.28 is good estimate of σ, how many replicate measurement should be made in order for the mean for the analysis of sample to be within 0.2% of the true mean 90% of the time.(5) A sample of sodium phosphate is dissolved in water to give 100.00 mL of solution (Solution A). Then this solution is diluted 5 times to give the final solution (Solution B). Solution B is Known to contain 3.920 x 1022 number of PO43- ions, which has an absorption peak at 460 nm and absorbance value of 0.355 in a 1.000 cm cuvette. (i) Calculate the molar absorptivity of Solution B. (ii) What mass of sodium phosphate (MM 163.94 g/mol) dissolved in Solution A.A student prepared four standard solutions of (NH4)2Fe(SO4)2 and measured their absorbance at 505 nm. She created a calibration plot with the best-fit line of y = 9372 x + 0.0539. She measured the absorbance of her diluted unknown sample solution as (4.69x10^-1) nm. If she prepared her diluted sample solution by diluting 10.00 mL of the original solution to a total volume of 50.00 mL with deionized water, what is the concentration of Fe2+ in her original solution? Answer in units of M. Note: Your answer is assumed to be reduced to the highest power possible.
- A 2.50 mL aliquot of a solution that contains 3.85 ppm Fe(III) is treated with an appropriate excess of KSCN and diluted to 100.0 mL. What is the absorbance of the resulting solution at 580 nm in a 0.50 cm cell? (Molar absorptivity of Fe (SCN)2+is 7.0 x 105L mol-1cm-1).Q4 (a) Analyze the importance of dropping mercury electrode on polarography. (b) (i) Calculate the molarity of MgSO4 in a solution containing 1.5 g ofMgSO4 in a volume of 250 mL?(ii) Calculate the weight of MgSO4 in grams which is present in 100mL of 0.076 M MgSO4?(c) Evaluate the key differences between paper chromatography and gaschromatographyA 5.00×10−4 M solution of analyte is placed in a sample cell that has a pathlength of 1.00 cm. At a wavelength of 490 nm, the solution’s absorbance is 0.338. What is the analyte’s molar absorptivity at this wavelength?
- (d) 3-13. Distis me Jum 4 A method of analysis yields weights for gold that are low by 0.4 mg. Calculate the caused by this uncertainty if the weight of gold in the sample is (a) 900 mg. (c) 150 mg. 1-7. The method described in Problem 3-6 is to be used for the analysis of ores that assay about 1.2% gold. What minimum sample weight should be taken if the relative error resulting from a 0.4-mg loss is not to exceed -0.2%? percent relative error (a) (b) (b) 600 mg. (d) 30 mg. 3-14. Wha stan stam 3-15. Сог mea (b) -0.5%? (a) -0.8%? (c) (d) 1.2%? 3.5 3-8. The color change of a chemical indicator requires an overtitration of 0.04 mL. Calculate the percent relative error if the total volume of titrant is (a) 50.00 mL. (c) 25.0 mL. 3-9. A loss of 0.4 mg of Zn occurs in the course of an analysis to determine that element. Calculate the per- cent relative error due to this loss if the weight of Zn in the sample is (a) 40 mg. (c) 400 mg. 3.1 3.1 (b) 10.0 mL. 3.3 2.5 (d) 40.0 mL. Fo (a (E (b) 175…Suppose that you are trying to measure the concentration of SO2 in air. To do that, you followed the para-rosaniline method. The SO2 was collected in a 10-ml solution of HgCl4 2- then diluted to 25 ml after the addition of the appropriate reagents. The absorbance owas measured at 650 nm in a 2.0-cm cell, yielding a value of 0.535. A standard sample was prepared by substituting a 1.00 mL sample of a standard solution containing the equivalent of 15.00 ppm SO2 for the airsample. The absorbance of the standard is found out to be 0.191. Report the concentration of SO2 in the air in parts per million. The density of air is 1.19 g/L2. Calculate the minimum concentration (µg/ml) of bismuth(III) (M=208.98 g/mol) in the analyte, which can still be determined by photometric method using the reaction with thiocarbamide, if the photometric measurements of the solution is carried out in a cuvette with a thickness of the absorbing layer = 1.00 cm, and the minimum value of the Absorbance measured by the spectrophotometer is 0.01. Molar attenuation coefficient = 9,1-10³ mol¹ L cm
