2. Show the curved arrow mechanism and predict the major product. Label the bonds responsible for the product peaks listed in the IR or the hydrogens responsible in the 1H NMR. Product IR (cm³) = 3230 1H NMR (1.4 ppm bs, 2H) and 3360 (both broad). 1. LiAlH (xs) ΝΗΣ 2. H₂O
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- 5. A compound having molecular formula C,H,OS reacts with hydrazine hydrate forming a product C with molecular formula C₁H,N₂S₂. The ¹H-NMR and ¹C-NMR spectra of the product is given below. Identify compounds A and C. Also, assign each NMR peak. Answer as soon as possible within 10 minutes with proper explanation in handwritten form. Don't answer after 11:58 PM Otherwise I will downvote and report !! Thank you5 (d) In the following reaction sequence (it is not necessary to explain the chemistry), what significant spectrum (i.e. before and after the reaction)? changes would you expect to see in the Infra-red spectrum and the 1C NMR OH 1) CH MgBr CH3 2) H,0+ The following four molecules are isomers, whose containers have lost their labels. Explain how the infra-red (IR) spectra and C NMR spectra could be used to distinguish between any TWO of these molecules. 4(d) 13 HC= HO. H3C CH3 но HO. II IV IIAnalysis of 1 5-bis(4’-methoxyphenyl)-1 4-pentadien-3-one by NMR. Please label the chemical shift (ppm), integration, splitting (single, doublet, triplet), and fragments (C-C). Is the C double bond C cis or trans?
- Based on this 1H-NMR what are the relevant peaks?Consider the product below a) Predict the 1H NMR spectrum for this molecule. Predict the multiplicity, integration and relative ppm b) Predict the 13C NMR spectrum and DEPT spectra. Use (+) for positivesignals, (-) for negative signals, and (X) for no signal in the DEPT NMR spectra.Please identify compound 1 and compound 2!!! Attached is the H-NMR and IR for both compounds (ignore the IR peaks ~2400). The experimental melting point for the aqueous layer was 260-261 celcius. The experimental melting point for the organic layer was 76.9-78.7 celcius. The following was my procedure: IntroductionThe reaction mixture in this experiment contains 4-bromobenzaldehyde, methanol, and aqueous potassium hydroxide. A reaction occurs that produces two organic compounds, compound 1 and compound 2. Both are solids at room temperature. Your task is to isolate, purify, and identify both compounds. A specific procedure is given for preparing the compounds, but you will need to work out the procedures for most other parts of this experiment.Experimental ProcedureThis procedure should produce enough of each compound to complete the experiment; however, in some cases, it may be necessary to run the reaction a second time. Although this experiment can be done individually, it works…
- A. Below is a “Name Reaction” - Clemensen reduction. Describe how the IR spectrum could be used to tell if the reactions had been successful. Provide approximate wave numbers and the corresponding functional groups for the key absorption bands and/or peaks in IR. You might want to describe from two aspects: which peak(s) of what functional group(s) should appear in the IR of the product (that is different from the reactant); which peak(s) of what functional group(s) should disappear in the IR of the product (that is present in the reactant B. For the Clemensen reduction (same reaction), describe how the 1H NMR spectrum could be used to tell if the reactions had been successful. Provide approximate chemical shifts and the integral and the “splitting” of the “unique” in the NMR spectrum. You might want to describe from two aspects: which peak(s) should have a change in chemical shift(s); which peak(s) should have a change in integral; which has a splitting change; which peak(s) will be…What is the 1H NMR data (chemical shift, integration, mulitplicity) of the compound shown below? Clearly label all hydrogens that are being reported.19. For the following reaction, which of the following change(s) in the IR spectrum is consistent with conversion of the reactant to the product? DMSO A. absorption at 3200-3600 cm should disappear B. absorptions at 3200-3600 cm and 1100 om should disappear C. absorption at 1100 cm should disappear, a new absorption at 3100 cm should appear D. absorption at 1720 cm should appear, absorption at 3200-3600 cm should disappear E. none of these O A O B O D O E
- 8 8. Correlate each signal in the following 'H NMR for ethyl cinnamate with a particular set of hydrogens. Be sure to explain the location of the signal, the integration pattern, and the splitting pattern for all peaks. 'H NMR (300 MHz, DMSO): 1.21 (3H, t), 4.06 (2H, q), 6.31 (1H, d), 7.48 (1H, d), 7.33 (1H, t), 7.38 (2H, m), 7.54 (2H, d). 7 6 5 4 PPM 3 2 1 X 0Provide the complete mechanism using CAF for the reaction shown below. Tell how many signals are visualized in the 1H spectrum for the starting material and the product. H₂O, H₂SO4 gr=gr NH₂ heat OH + NH4+ HSO4Predict (draw) the ¹H NMR and 13C NMR spectra for each molecule. Your illustration should include chemical shift, integration, and splitting (where appropriate). Label each signal in your spectrum a, b, c... etc and label the corresponding C/H atoms in each molecule. CI