MTSE 6600 Assignment #1:
TEM Components and Alignments
Name: Tianhao Wang
Components:
Vacuum System:
#1: What is the difference between a gas transfer and a gas entrapment vacuum pump?
Answer: A Gas Transfer Vacuum Pump will move the molecules out of the system so that the vacuum environment is formed. And an Entrapment Vacuum Pump will trap the molecules in some way, and they can’t move freely any longer so that the vacuum environment is formed.
#2: What are the two types of gas transfer pumps?
Answer: (1) Positive Displacement Pumps and (2) Kinetic Vacuum Pumps.
#3: Describe how any two types of vacuum pumps work.
Answer:
(1)The Positive Displacement Pump:
The Positive Displacement Pump exhausts a certain volume of gas successively to reduce the pressure of a system and creates a partial vacuum. The schematic diagram is shown below. (Source: Basic Vacuum Practice, 3rd Edition, Varian Vacuum Products.)
(2) Ion Getter Pump:
First, Gases are ionized which will be trapped to the cathode. Then the sputtered Ti atoms will cover the gas ions trapped on the cathode. Thus, this chemisorption is completed. The schematic diagram is shown in next page.
(Source: http://www4.nau.edu/microanalysis/Microprobe-SEM/Images/Ion_Pump_Operation.jpg)
#4: Give two reasons why we want to have a good vacuum in the TEM. Briefly describe the importance of these two reasons.
Answer: (1) The increase of the mean free path and (2)
A sample of gas is trapped in a sealed container, which has a movable lid. Moving the lid up or down will change the volume inside the container. You will use an attached manometer to measure the pressure inside the container.
Once inverted, built-up gas was released by turning the stopcock to its opened and closed positions. This was repeated for about four times in one minute intervals. Then the layers were allowed to settle until a separation between liquids could be observed. Due to the low density of the product, the top layer was to be extracted. The bottom layer was carefully and slowly extracted out of the separatory funnel.
Emmanuel and his mother live in an urban community-housing complex. The building is worn down and dirty from the urban dust, cockroaches, and mold. Emmanuel is five years of age and has suffered from asthma for the last two years. One evening, his mother poured him some milk and put him to bed. Shortly afterward, Emmanuel woke up wheezing and coughing. As he gasped for air, he became more and more anxious. His mother ran for his inhaler, but he was too upset and restless to use it. Emmanuel’s skin became moist with sweat, and as he began to tire, his wheezing became quieter. His mother called 911 and waited anxiously for the ambulance to arrive.
-If the potassium transport pump was blocked the leakage channels would still be open allowing Na+ to
On 01/08/2015, at approximately 0930 hours, your affiant was dispatched to the area of the Valero gas station. The reporting person informed the dispatcher that there is a truck parked in the road blocking traffic and the driver is slumped over the steering wheel.
How is it possible to have gas trapped in the table? (Is it really trapped or is it a product?)
Diffusion and osmosis happens in everyones everyday way of living, this can include when you spray your deodorant before school in the bathroom to then find going into the next room your still chocking on the dry smell of the deodorant this is diffusion when the particles in the air move from one place to another. Other example is when you go to have a bath, you fill the water put a bath bomb in the water and go get your towel and clothes when you get the bath bomb is gone but some little piece may be left over this is Osmosis this happens when two different concentrated solutions are separated then the solvent will then diffuse by the membrane from the less concentrated solution over to the more concentrated solution,
5.Position gas collecting hose so it runs from reaction vessel through gas collecting box to opening of the graduated cylinder. The idea is that any gas coming through the tube will rise in the graduated cylinder and displace the water in it.
Small pockets of the specific liquid, that contains trapped gas, that is then released to the
The SiF4 is removed from the gas stream by contacting the gas with water droplets. This water hydrolyses (hydrolyses is chemical decomposition in which a compound is split into other compounds by reacting with water), (Dictionary.com 2015) the SiF4 as follows (Chemprocess 2015):
1) What happens to the vapor pressure of water after the heat source is removed? What observation is proof of this? After the heat source was removed, the vapor pressure was decreased. This is proven by the boiling stopping.
The purpose of this experiment was to test and observe the physical and chemical properties of gases, and to use these properties to identify these gases when they are encountered.
In step 4e, pour the solution into the "+air" bottle and cap it, placing the open end of the collection tube inside the gas collecting
process takes place for horizontal pipeline, that is responsible for collecting the natural gases. A
30. Same as carried out in Part (b), repeat steps 18. to 24. to dissolve the gas in the syringe in the heated de-ionised water.