Lab 2. The Gravimetric Determination of Chloride in a Soluble Sample Introduction: For the experiment you will obtain an unknown sample, containing chloride ion, and perform the gravimetrical procedure using the sample of the analyte. An analyte is a chemical constituent that is determined from analytical techniques. The technique used in the experiment is the gravimetric determination analysis which is a method of quantitative chemical analysis in which the key constituent being sought after is converted to a substance that can be separated from the remaining sample. A common method for determining chloride ions involves isolating the silver chloride precipitate via filtration, determining its mass, and using stoichiometry to …show more content…
(Average % Cl- in the sample and standard deviation: 55.84 +/- 2.7381) CHEMICALS USED .2M=(x/169.8747)=33.97494g of AgNO3 1. (.1437g of NaCl) 2. (.1430g of NaCl) 3. (.1425g of NaCl) Grams of NaCl are dissolved in 100ml of Di-water Discussion: The chemical reactions began after all the
In this Chemistry Lab the main objective is to perform accurate chemical analysis for the quantity of elements and compounds in a sample. There will be a compound made then synthesized. The methods used were acid-base titrations, redox titrations, gravity filtration, and distillation. General conclusions included
The objective of this lab was first to convert the mass of a compound to the number of moles and number of molecules and then determine the concentration of salt and its component. The first thing we did was get the mass of an empty container by using a scale and it came out to be 16.87g. Next thing we did was pick a substance which in this case it was Potassium Chloride and placed it on the scale to get a total mass of 31.20g. The container the Potassium Chloride was in only had a mass of 16.87g which means that the mass of the substance was 14.33g. To convert the mass to the number of moles we took the amount of the substance 14.33g and divided it by the mass of Potassium Chloride 74.55g and figured out that the number of moles was 0.192.
To begin the procedure of the gravimetric analysis of chloride, 0.501g of Amine (C8H9NO) was weighed on an analytical balance and added to a 10mL volumetric flask. At this point 5mL of deionized water was added to dissolve the Amine. Then 5mL of 1 M AgNO3, which was already combined with 4 M HNO3, is added to the 10mL volumetric flask and stirred. To collect the AgCl precipitate,
The wet, crude product was placed into the 50 mL Erlenmeyer flask. Small amounts of CaCl2 were added to dry the solution. The flask was sealed and the mixture was swirled and left to settle. Once
Obtain a ring stand, ring, and wire clay triangle to heat the sample. Measure the mass of a crucible and its cover. Measure the mass of the copper chloride hydrate. Record both masses. Next, pour the hydrate into the crucible and measure and record the mass with the crucible lid on. Place the crucible on the clay triangle, tilting lid slightly away from you to prevent inhaling or coming in contact with any fumes that the compound may
First, we were to measure and record the mass of a beaker, then transfer about 1 gram of the salt mixture into the beaker, measure, and record the combined mass. Then, we had to fill a 400-ml beaker with deionized water and test it to make sure that the ph was just basic. We then combined the deionized water and salt by adding about 150ml of the deionized
It used mass, temperature, length, volume, density, and making a dilute solution. I learned the importance as well as the difficulty of making proper measurements in a lab setting. If one measurement is off, it will throw the entire equation off. This will give either incorrect or inaccurate results.
The purpose of this lab was to become familiar with the three different balances and two different methods used to find the weight and mass of chemicals and compounds in the ChemLab program. The lab was performed by using three different types of balances, and the direct weighing and weighing by difference methods.
of being able to analyze multiple samples in a short amount of time. The most efficient way of determining concentration is to prepare a set of standard solutions of known
Gravimetric analysis is a quantitative (i.e. how much?) method of classical analysis. The element to be determined is isolated in a solid compound of known identity and definite composition. The mass of the element that was present in the original sample can be determined from the mass of this compound.
The weight of each 50ml beaker (used for weighing the mass of dissolved Potassium chloride after the evaporation of water) should be recorded. If the experimenter were to weigh the mass of one beaker and take it as a default mass, the latter may be a source of error.
For my Senior Project, I am submitting a lab which I completed in AP Chemistry. In the Gravimetric Analysis of Calcium and Hard Water Lab my lab partner and I conducted an experiment in which we calculated the mass of the precipitate formed by the mass of the isolated analyte present in the reactants before the reaction. During our experiment, we used resources such as graduated cylinders, sodium carbonate, bunsen burners, an analytical balance, watch glass, filter paper, a funnel, tongs, and an oven. The lab equipment allowed us to effectively precise measurements of water hardness. For example, the analytical balance gave us a more precise measurement than a triple beam balance would. The temperature of the burners as well as the temperature
In this lab, "Gravimetric Methods," students were expected to be able to calculate the mass percentage of an unknown hydrate, describe the process of gravimetric analysis, and put together the equipment needed to evaporate water from the unknown hydrate. Gravimetric analysis is the process in which an amount of a substance can be found by measuring the mass. By comparing the masses of two compounds that contain the substance, one can successfully complete a gravimetric analysis. The initial recorded mass will be different from the final recorded mass since part of the substance evaporates from the container. By subtracting the initial mass from the final mass, students can determine the amount of the substance that evaporated. They can
The main objective of this experiment is to carry out qualitative analysis to identify metal cations in unknown solution 1.
Analysis mode: The procedure is done to estimate different types of molecules and their individual quantities in the mixture using the help of a detector.