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Calorimetry Lab

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In order to conduct the experiment, the first step is to measure the aluminum pieces in a tared weigh boat in which the mass lies in between 0.9 to 1.2 grams then transfer them into a 250mL beaker. Then, pour the 50 mL of 1.4 molarity of potassium hydroxide into the 250mL beaker with the aluminum pieces as it’s on the hot plate. Thirdly, set up the aspirator and connect it to the apparatus; then apply a damp filter paper to the büchner funnel when the solution is completely done mixing with the aluminum pieces. Turn on the vacuum and pour the solution through the filter. Once, that is complete, move the filtrate to a clean 250 mL beaker and clean the flask using 10 mL of distilled water and emerge the clean flask with the filtrate. Add three-fourths of ice to the …show more content…

Afterwards, place the reaction beaker in the ice beaker. Meticulously pour 20mL of 6.0 sulfuric acid in the reaction beaker slowly as well as stirring it consistently. If solids form within the beaker, place the beaker on the hot plate in order to break down the solids and maintain its state. Keep adding ice until the reaction beaker does not have any solids. This will help the alum precipitate and eventually form alum crystals. Then use a scoopula to scratch the bottom of the reach beaker to help the alum crystals maintain shape. Once the reaction beaker is done forming the alum crystals, sterilize and put together the vacuum filtration apparatus. Then transfer the alum crystals onto a new filter paper. After that, the beaker is consumed twice with 10mL of 50 percent of the ethanol solution. The alum crystals on the filter paper are filled with the 10mL of ethanol as well as using the vacuum to dry the alum crystals. As the crystals are drying, obtain the weight of the watch glass to the nearest 0.0001 grams. The alum crystals that are on the filter paper are transferred to the watch glass in order to receive the mass of the

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