Concept explainers
(a)
Interpretation:
A standard-addition plot should be created using the data given.
Concept introduction:
A commonform of standard-addition method involves adding known amounts of a standard solution to sample aliquots containing a fixed volume. Measurements taken for each solution can be used to plot a standard-addition plot.
(b)
Interpretation:
Using the standard-addition plot constructed, the concentration of the unknown phenobarbital sample should be determined.
Concept introduction:
In a standard-addition plot, the graph can be extrapolated to obtain thevolume of standard reagentequivalent to the amount of analyte in the sample (
Where,
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