This method is to be used when measuring the volume of a solution containing sufficient reagent to react completely with the analyte. Volumetric O Spectroscopic O Gravimetric Electroanalytical
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- A clinical chemist obtained the following data for the alcohol content of a sample of blood: % C,H OH: o.084, 0.089, and o.079. Calculate the 95% confi- dence interval for the mean assuming that (a) the three results obtained are the only indication of the precision of the method and that (b), from previousWhat is precipitation from homogeneous solution; what are the benefits of this method.Briefly explain the principles involved in the separation of the components of a mixture by solvent extraction.
- In the Analytical Chemistry laboratory, one of the B.Sc student Ms. Fatma wanted to analyze the presence of Iron(II) ion in the water samples collected from Sohar Industrial Area in the Sultanate of Oman and analyzed by Spectrophotometric method. (1) 250.00 mL of this water sample (Solution A) known to contain unknown amount of FeSO4. She has diluted Solution A by a dilution factor 10 to make 250.00 mL solution, which she labeled Solution B. Using Spectrophotometer, she has measured the absorbance value (0.642) for Solution B at 508 nm using 1.00 cm cell (cuvet). The molar absorptivity value for Fe2* ion at 508 nm is ɛ508 = 30.8 M-1cm1. (i) What volume of the solution A did she require to make the 250.00 mL of Solution В? (ii) in (i)? What instrument should she use to transfer the volume of the Solution A calculated (ii) Concentration of FeSO4 in Solution B. (iv) Concentration of FeSO4 in Solution A. Mass of FeSO4 in Solution A (Show your calculation) (v)What are the advantages and disadvantages of volumetric and gravimetric analysis?(i) (ii) (iii) (iv) 'I OMe HO H g H N Me Br SnMe3 OSiMe3 CHO OH NaNH, NH3 (1) Phl, Pd(PPH3)4 THF, reflux 1. Ph3P=CMe2 2. "Bu4NF 3. H30 + CH₂12, Zn C C₂H₂NO D C₁1H₁1N E C10H16O F C15H26O2
- Hexanoic acid was added to an immiscible biphasic solvent sysem, water and CCl4 at 20.0OC and the equilibrium concentrations of hexanoic acid were determined to be 3.66 g/L in H2O and 67.0 g/L in CCl4. Caluclate the distrubution coeffiecent (D1) of hexanoic acid in CCl4 with respect to water.50.00 cm3 of a 1.5784 mol.dm-3 solution of potassium hydroxide is transferred to an empty 700.00 cm3 volumetric flask. This flask is made up to the mark with distilled water and then shaken well. The concentration of the potassium hydroxide in this second flask is:The air in a recently used classroom 9m x 7m x 9m tested 0.12% carbon dioxide. How many cubic meters of fresh air must be admitted per minute in order that 10 minutes later it shall contain not over 0.06% carbon dioxide. Fresh air contains 0.04% carbon dioxide. Assumeimmediate mixing of fresh with stale air. (A) 14 (B) 11 (C) 15 (D) 19 (E) 17
- 3.) The following Beer's Law calibration plot was collected at 391.9 nm using the five mixtures listed above. The trendline equation was y = 4617.1x. A saturated solution of lead(II) chromate had an absorbance of 0.0025. Calculate its solubility, in molarity. Molar Solubility of PbCrO4: x 107 M ABSORBANCE VS CHROMATE CONCENTRATION AT 391.9 NM 1.40 1.20 y = 4617.1x R-0.9972 1.00 0.80 0.60 0.40 0.20 0.00 C 0.00005 0.0001 0.00015 0.0002 0.00025 0.0003 Chromate concentration (mol.L)* The indicator of Moher regent is KCr04. KMN04.Calculation of the volume of 1.25 M NaOH (aq.) required to extract 1.0 gram of 2-naphthol. Use 20% mole excess of NaOH (i.e. use 1.2 mol of NaOH for every 1 mol of 2-naphthol).