One of the problems that can be encountered in recrystallization is the failure of the solute to crystallize. In which of the following scenarios could that happen? a. Cooling the filtrate in an ice bath. b. Using a wide bore, long-stemmed funnel in the hot filtration step. c. Addition of too much water in the receiving flask. d. Washing the residue with cold solvent

One of the problems that can be encountered in recrystallization is the failure of the solute to crystallize. In which of the following scenarios could that happen? a. Cooling the filtrate in an ice bath. b. Using a wide bore, long-stemmed funnel in the hot filtration step. c. Addition of too much water in the receiving flask. d. Washing the residue with cold solvent

Introductory Chemistry: An Active Learning Approach

6th Edition

ISBN:9781305079250

Author:Mark S. Cracolice, Ed Peters

Publisher:Mark S. Cracolice, Ed Peters

Chapter16: Solutions

Section: Chapter Questions

Problem 16.3TC

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2. When performing the recrystallization of an impure solid, why is it advised to use the minimal amount of solvent possible? Group of answer choices To minimize the amount of pure solid lost due to its solubility. To minimize the cost of the recrystallization. To reduce the time needed to filter the pure solid from the solvent after recrystallization. To minimize the amount of hazardous materials used.
In recrystallization, is it always good to have a high % recovery? Explain. What are the advantages and disadvantages of recrystallization?
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Why is recrystallization not applicable to samples which contain large amount of impurities?
The solubility of benzoic acid in water is 0.21g per 100mL of water at 10 degrees celsius, 0.27g per 100mL at 18 degrees celsius, and 6.80g per 100mL at 95 degrees celsius. A. At least how much water would be needed to dissolve a 2.00g sample of benzoic acid at 95 degrees celsius? B. If you carried out a recrystallization by dissolving your 2.00g sample in water at 95 degrees celsius, then cooling it to 18 degrees celsius, what would be the maximum yield of benzoic acid? How would the yield be affected if the recrystallization mixture was cooled to 10 degrees celsius instead?
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