O 4000 100 80 60 IR Spectrum (liquid film) 40 20 v (cm') 87 M = 146 (<1%) 40 80 120 160 m/e 13C NMR Spectrum (20.0 MHz, CDCI, solution) proton decoupled 200 ¹H NMR Spectrum (100 MHz, CDC1, solution) 9 % of base peak 10 3000 43 134 8 1760 C 2000 1600 160 200 120 1200 800 Mass Spectrum 240 C6H1004 280 C-H solvent JIL 80 the 1 7 6 5 4 Problem 45 No significant UV absorption above 220 nm -CH₂ -CH₂ TMS 08 (ppm) TMS 0 8 (ppm) 40 3 2 1

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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What is the IR and HNMRAndCNMR and mass
O
4000
100
80
60
IR Spectrum
(liquid film)
40
20
v (cm')
87 M = 146 (<1%)
40
80
120 160
m/e
13C NMR Spectrum
(20.0 MHz, CDCI, solution)
proton decoupled
200
¹H NMR Spectrum
(100 MHz, CDCI, solution)
9
% of base peak
10
3000
43
134
8
1760
C
2000
1600
160
200
120
1200
800
Mass Spectrum
240
C6H1004
280
C-H
solvent
Jill
80
the
1
7 6 5 4
3
Problem 45
No significant UV
absorption above 220 nm
-CH₂
40
11
-CH₂
TMS
08 (ppm)
TMS
0
8 (ppm)
2 1
Transcribed Image Text:O 4000 100 80 60 IR Spectrum (liquid film) 40 20 v (cm') 87 M = 146 (<1%) 40 80 120 160 m/e 13C NMR Spectrum (20.0 MHz, CDCI, solution) proton decoupled 200 ¹H NMR Spectrum (100 MHz, CDCI, solution) 9 % of base peak 10 3000 43 134 8 1760 C 2000 1600 160 200 120 1200 800 Mass Spectrum 240 C6H1004 280 C-H solvent Jill 80 the 1 7 6 5 4 3 Problem 45 No significant UV absorption above 220 nm -CH₂ 40 11 -CH₂ TMS 08 (ppm) TMS 0 8 (ppm) 2 1
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