Melting point range Recrystallized Phenacetin 95-100 Recrystallized Phenacetin + Reference Phenacetin 110-115 Recrystallized Benzil 92-95 Recrystallized Benzil + Reference Benzil 94-98   Questions: 1.  What does your melting point say about the purity of your phenacetin sample?  Justify your answer using the characteristics of mixed melting point.   2.  What does your melting point say about the purity of your phenacetin sample?  Justify your answer using the characteristics of melting point.   3.  What are two characteristics of a good recrystallization solvent for a given compound?   4. Given a solid sample that contains impurities, how would you determine which solvent to use for a recrystallization?  Describe how you would do this in the laboratory.   5. Clearly explain the difference between a recrystallization and a precipitation.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Melting point range

Recrystallized Phenacetin

95-100

Recrystallized Phenacetin + Reference Phenacetin

110-115

Recrystallized Benzil

92-95

Recrystallized Benzil + Reference Benzil

94-98

 

Questions:

1.  What does your melting point say about the purity of your phenacetin sample?  Justify your answer using the characteristics of mixed melting point.

 

2.  What does your melting point say about the purity of your phenacetin sample?  Justify your answer using the characteristics of melting point.

 

3.  What are two characteristics of a good recrystallization solvent for a given compound?

 

4. Given a solid sample that contains impurities, how would you determine which solvent to use for a recrystallization?  Describe how you would do this in the laboratory.

 

5. Clearly explain the difference between a recrystallization and a precipitation.

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