Match the compound to spectrum by drawing the structure next to correct spectrum. Then explain by describing the total number of signals each structure should have and which carbon would be farthest downfield. CH3(a) (CH3)2CHCH,OH(b)`CH3(c)(d)(e)CHCH3Spectrum ASpectrum BTMSTMSCDC,220 200 180 160 140 120 100 806008220 200 180 160 140 120 10080604020Chemical shift (ppm)Chemical shift (ppm)Spectrum CSpectruin DTMSTMSCDCI,mimmm pmm m220 20020 200 180 160 140 120 100806010 20180 160 140 120 1006090402008Chemical shift (ppm)Chemical shift (ppm)in Spectruim ETMSCDCI,.220 200 180 160 140 120 100 806040 2008Chemical shift (ppm)

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Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

ChapterL3: Carbon (13c) Nmr Spectroscopy

Section: Chapter Questions

Problem 9CTQ

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Match the compound to spectrum by drawing the structure next to correct spectrum. Then explain by describing the total number of signals each structure should have and which carbon would be farthest downfield.

CH3
(a) (CH3)2CHCH,OH
(b)
`CH3
(c)
(d)
(e)
CH
CH3
Spectrum A
Spectrum B
TMS
TMS
CDC,
220 200 180 160 140 120 100 80
60
08
220 200 180 160 140 120 100
80
60
40
20
Chemical shift (ppm)
Chemical shift (ppm)
Spectrum C
Spectruin D
TMS
TMS
CDCI,
mimmm pmm m
220 200
20 200 180 160 140 120 100
80
60
10 20
180 160 140 120 100
60
90
40
20
08
Chemical shift (ppm)
Chemical shift (ppm)
in

Spectruim E
TMS
CDCI,.
220 200 180 160 140 120 100 80
60
40 20
08
Chemical shift (ppm)

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