Immiscible Liquid-Liquid Extraction: A feed of 13,500 kg/hr consists of 8.0 wt% acetic acid in water. The removal of acetic acid is to be accomplished by liquid-liquid extraction in water at 25°C. The raffinate is to contain no more than 1.0 wt % acetic acid. SOLVENT K The following four solvents (and accompanying distribution coefficients are being considered. Water and each solvent can be considered immiscible. Methyl acetate Isopropyl ether Heptadecanol Chloroform 1.273 0.429 0.312 For each solvent, estimate the flow rate (kg/hr) if a single equilibrium stage is used to achieve the desired separation. 0.178 Discuss the solvent choices and indicate which may be the best option.

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Publisher:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Chapter1: Introduction
Section: Chapter Questions
Problem 1.1P
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Immiscible Liquid-Liquid Extraction: A feed of 13,500 kg/hr consists of 8.0 wt% acetic acid in water. The
removal of acetic acid is to be accomplished by liquid-liquid extraction in water at 25°C. The raffinate is to
contain no more than 1.0 wt % acetic acid.
SOLVENT
K
The following four solvents (and accompanying distribution
coefficients are being considered. Water and each solvent can be
Methyl acetate
Isopropyl ether
Heptadecanol
Chloroform
1.273
0.429
considered immiscible.
0.312
For each solvent, estimate the flow rate (kg/hr) if a single
equilibrium stage is used to achieve the desired separation.
0.178
Discuss the solvent choices and indicate which may be the best option.
Transcribed Image Text:Immiscible Liquid-Liquid Extraction: A feed of 13,500 kg/hr consists of 8.0 wt% acetic acid in water. The removal of acetic acid is to be accomplished by liquid-liquid extraction in water at 25°C. The raffinate is to contain no more than 1.0 wt % acetic acid. SOLVENT K The following four solvents (and accompanying distribution coefficients are being considered. Water and each solvent can be Methyl acetate Isopropyl ether Heptadecanol Chloroform 1.273 0.429 considered immiscible. 0.312 For each solvent, estimate the flow rate (kg/hr) if a single equilibrium stage is used to achieve the desired separation. 0.178 Discuss the solvent choices and indicate which may be the best option.
-100
Water
Glycol-
100-
10
Raffinate'
20
-Furfural-
-Glycol 100
70
Extract
-0-
0-
10
001-
-Furfural 0
08
OL
09
Water
Water
00L
09
06
06 V
R
08
lines
Furfural
09
E,
Os
APlait point7
09
50,
06
glycol
Ethylene
Transcribed Image Text:-100 Water Glycol- 100- 10 Raffinate' 20 -Furfural- -Glycol 100 70 Extract -0- 0- 10 001- -Furfural 0 08 OL 09 Water Water 00L 09 06 06 V R 08 lines Furfural 09 E, Os APlait point7 09 50, 06 glycol Ethylene
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