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- A) Phenol Red is a weakly acidic dye which is yellow in the HA form and red in the A form. What concentration of Phenol Red is required to obtain an absorbance of 0.50 at 550 nm at pH 7.8? Note: ε550 of A = 2.5 x 104 M-1 cm-1; ε550 of HA = 0; pKa = 7.8. B) What would the absorbance of the solution in part (a) be if the pH was 8.8?Please provide the IUPAC name (only) for the compound that best represents the spectroscopic data here: • Molecular formula: C4H100 Important IR data (cm 1): 3280 (broad); 2910-2950 (many); 1053 • All 'H NMR data shown as x.xx ppm (splitting), integration. 1.23 ppm (t), 3 1.23 ppm (d), 3 "-OH" 1.46 ppm (m), 2 4.03 ppm (m), 1 5. PPMTo trans-[COC12(en)2]ci Annotate the NMR of trans-[CoCl2(en)2]Cl on the top and cis-[CoCl2(en)2]CI on the bottom -5.955 -5.677 -5.245 4.381 -5.189 E96'E- - 3.424 – 3.686 -2.766 -2.785 -2.639 -2.301 -1.033
- Draw the structure of the compound that produced the spectra below. The infrared spectrum has strong bands at 1720 and 1738 cm-1.6. (Chapter 15 - 47b) An aromatic compound, C9H12 has the following H NMR spectrum and a peak at 750 cmt in its IR spectrum. Answer the following questions. Chem. shift Rel. area 1.19 2.31 2.64 7.13 1.50 1.50 1.00 2.00 TMS 10 3 O ppm Chemical shift (6) 4(a). The IR peak at 750 cm in its IR spectrum indicate that the compound is. disubstituted = 4(b) The name of the compound is = Intensity-1.1.1 2.1 3 1.4.1 5 1·6·1 7.1 8 9.1. 10.1 11. 12. 1 1B The following spectra for A and B correspond to two structural isomers with a molecular formula of C.HnN. The NMR singlet at 81.16 in spectrum A disappears when the sample is shaken with Dr0. The singlet at 80.60 ppm in the spectrum of B disappears on shaking with D20. Propose structures for these isomers, and explain how it is consistent with the observed absorptions. 2. 1. wavelengih (am) 3.5 6 100 25 3.5 4 4.5 $ 9 10 12 13 14 1S 16 m 80 60 40 AW 20 4000 3500 3000 2500 IKI SIKI wanenumber icm 200 180 160 140 120 60 40 在 %3D
- Absorbance 7. Compound 7 is a neutral, low-melting solid (mp - 22.24°C) Elemental Analysis: C-72.00%, H-6.67%, O-21.33% "C Spectral Data: 196.5ppm(s), 166.4ppm(s), 129.7ppm(s), 129.6ppm(d), 114.0ppm(d), 56.0ppm(q), 22.8ppm(q) Mass Spectrum Compound 7 Structure W Inlanalty Infrared Spectrom 4000 3000 2500 1 'H NMR 20 100 110 120 130 140 150 100 170 100 100 201 Wave Number, am 1600 1300 1300 1100 130 Wavelength, microns 700 CHEM 241L Exp#12 NMR Spectroscopy www................................. www. Ppm, 8 Rev. 052318JKOThe molecular formula of unknown compound B is C10H16.Quantitative brominationof a 0.473-g sample of compound Brequired 48.22mL of a 0.216MBr2/CCl4to produce a color change. How many rings and pi bonds does compound Bcontain?Include any explanations/calculations to justify your answers.Pls help identify these :(
- What compound is consistent with the NMR spectrum below? d6-DMSO solution F0.60 0.55 -0.50 -0.45 -0.40 -0.35 -0.30 -0.25 -0.20 -015 -0.10 -0.05 -0.00 0.05 6.5 5.5 5.0 4.5 4.0 6.0 f1 (ppm) 7.5 7.0 HOI HO. но но (A) (B) (C) (D) Forp-nitroaniline (2max : 375 nm) absorbs at a longer than Phitrobenzene (c) Explain why wavelength (hmax : 260 nm). (ij Write a short note on absorption. spectra complexes of charge transfer11 An unknown compound A has the molecular formula C12H16O. Compound A absorbs strongly in the IR at 1700 cm-1. The NMR spectral data for compound A are given below. What is the structure of compound A? A. absorption singlet triplet "ost of B. quartet broad singlet ppm 1.0 1.2 2.2 7.0 C. D. ratio of absorbing H's 6 325 2 the