Chemistry
Chemistry
10th Edition
ISBN: 9781305957404
Author: Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher: Cengage Learning
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Draw reaction mechanism for the synthesis of salicylic acid from oil of winter green. 
draw reaction mechanism for the synthesis of aspirin from salicylic acid. 

27
IUPAC
NAME
Exp. No.
Winter
green
Name
Procedures
10. Add 3.75mL of deionized
water per gram of solid. Heat
and continue to stir
11 transfer the beaker to a ice
bath. Isolate the product and
Suction for 10 minutes. transfer
the solid to a clean beaker and
even dry for 1-hour
the
12. Remove Cool and wigh
final product
13. In a test tube, add 0.25mL OF
ethyl acetate and add a spatela
tip amount of solid. Stir until it
Clissolves.
4. Using a pasteur pipet, transfer
4-5 drops of this solution to a
Salt plate and allow the solvent
to evaporate
Table of chemicals:
Structure CASH
10
Catherine traze
sodium
Hydroxide
delonized
water
Salicyclic
A cid
Experiment/Subject
Synthesis of Aspirin
Lab Partner
Signature,
он
M
0
Na-OH
н-о-н
0\
요 아
WOM
он
119-36-8132.15 220
°C
Observations
role
Molecular BP Mp Solubility Density Aman fok
use
Mass
in
g/mol
g/mL
c/ Water
OC
Graze
THE HAYDEN-MCNEIL STUDENT LAB NOTEBOOK
7732-18 18.015
-5
Date
03/27/2023
Locker/
Desk No.
1310-73-2 39.997 1388 323 very
ос
°C soluble
0
100 O
°C
24-72-71137
69-72-7 138.12 211
ос
Witness/TA
Course &
Section No. 5
-8.6 Slightly 1.174
°C Soluble
soluble
°C
138 soluble
OC
2.13
glmc
1.44
Date
IML
Note: Place fold-over back cover under copy sheet before writing
expand button
Transcribed Image Text:27 IUPAC NAME Exp. No. Winter green Name Procedures 10. Add 3.75mL of deionized water per gram of solid. Heat and continue to stir 11 transfer the beaker to a ice bath. Isolate the product and Suction for 10 minutes. transfer the solid to a clean beaker and even dry for 1-hour the 12. Remove Cool and wigh final product 13. In a test tube, add 0.25mL OF ethyl acetate and add a spatela tip amount of solid. Stir until it Clissolves. 4. Using a pasteur pipet, transfer 4-5 drops of this solution to a Salt plate and allow the solvent to evaporate Table of chemicals: Structure CASH 10 Catherine traze sodium Hydroxide delonized water Salicyclic A cid Experiment/Subject Synthesis of Aspirin Lab Partner Signature, он M 0 Na-OH н-о-н 0\ 요 아 WOM он 119-36-8132.15 220 °C Observations role Molecular BP Mp Solubility Density Aman fok use Mass in g/mol g/mL c/ Water OC Graze THE HAYDEN-MCNEIL STUDENT LAB NOTEBOOK 7732-18 18.015 -5 Date 03/27/2023 Locker/ Desk No. 1310-73-2 39.997 1388 323 very ос °C soluble 0 100 O °C 24-72-71137 69-72-7 138.12 211 ос Witness/TA Course & Section No. 5 -8.6 Slightly 1.174 °C Soluble soluble °C 138 soluble OC 2.13 glmc 1.44 Date IML Note: Place fold-over back cover under copy sheet before writing
NEM
SSSSS
Exp. No.
Name
10
Katherine Erazo.
Table of chemicals
IUPAC
Name
асенс
Anhydride (
oto
0.7mm
кон
Aspirin 04
Experiment/Subject
Synthesis of Aspirin
Lab Partner
Structure / Cas H
Q
вр
Molecular BP MP solubility Density
Mass
OC
10
g/mol
water
glm L
100-24-7 102.09
1.08
Po
139.5-73 soluble
o C
Jo.
50-76-2 170.16 140
03/27/2021
Locker/
Desk No.
Do
135
OC
Course &
Section No. 5
soluble 1.40
мине
pen
expand button
Transcribed Image Text:NEM SSSSS Exp. No. Name 10 Katherine Erazo. Table of chemicals IUPAC Name асенс Anhydride ( oto 0.7mm кон Aspirin 04 Experiment/Subject Synthesis of Aspirin Lab Partner Structure / Cas H Q вр Molecular BP MP solubility Density Mass OC 10 g/mol water glm L 100-24-7 102.09 1.08 Po 139.5-73 soluble o C Jo. 50-76-2 170.16 140 03/27/2021 Locker/ Desk No. Do 135 OC Course & Section No. 5 soluble 1.40 мине pen
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