Compound 47 is a high-boiling liquid (boiling point 204-205 'C), that reacts with Ag* ion in aqueous ammonia to form a "silver mirror" (the Tollens test). The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 79.97; H, 6.71; O, 13.32.

Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter14: Mass Spectrometry
Section: Chapter Questions
Problem 14.29P
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Compound 47 is a high-boiling liquid (boiling point 204-205 'C), that reacts with Ag* ion in aqueous ammonia to form a "silver
mirror" (the Tollens test). The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C,
79.97; H, 6.71; O, 13.32.
Transcribed Image Text:Compound 47 is a high-boiling liquid (boiling point 204-205 'C), that reacts with Ag* ion in aqueous ammonia to form a "silver mirror" (the Tollens test). The Mass, IR, and 'H NMR spectra, along with 13C NMR data, are given below. Elemental Analysis: C, 79.97; H, 6.71; O, 13.32.
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