Chemistry
Chemistry
10th Edition
ISBN: 9781305957404
Author: Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher: Cengage Learning
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i need help calculating the molar concentration for part C

**Experiment 35 Report Sheet**

**Spectrophotometric Metal Ion Analysis**

**Metal Ion for Analysis**

---

**A. A Set of Standard Solutions**

1. **Prepare a stock solution.** Show the calculation for the mass of metal ion salt in the preparation of the stock solution. Refer to Prelaboratory Assignment, question 2a.

   Calculation:  
   \[
   100\text{mL} \times 1\text{L} / 1000\text{mL} \times 0.10\text{mol} / 1\text{L} \times 249.68\text{g} = 2.5\text{g } \text{CuSO}_4\cdot\text{5H}_2\text{O}
   \]

   - **Measured tared mass of metal ion salt (g):** 2.499

   - **Description of the preparation of the 0.10 M stock solution.**

   - **Concentration of stock solution (mol/L):** 0.01 M

---

**B. Determination of \(λ_{max}\)**

2. **Wavelength Scan.** Use the following table to record the wavelength and absorbance data.

   | λ    | Abs | λ    | Abs | λ    | Abs | λ    | Abs | λ    | Abs |
   |------|-----|------|-----|------|-----|------|-----|------|-----|
   |      |     |      |     |      |     |      |     |      |     |

   - **Plot the data of absorbance versus wavelength to set \(λ_{max}\). From the data plot, \(λ_{max}\):** 610 nm

   - **Have the instructor approve your graph.**

---

**C. Plot the Calibration Curve**

1. **Absorbance of Standard Solutions.** Read and record the absorbance values for the standard solutions.

   | Standard Solution | Volume of Standard Solution (μL) | Absorbance | Calculated Molar Concentration |
   |-------------------|-----------------------------------|------------|--------------------------------|
   | Blank             | 0                                 | 0.033      |                                |
   | 1                 | 2                                 | 0.095      |                                |
   | 2                 | 5                                 | 0.763      |
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Transcribed Image Text:**Experiment 35 Report Sheet** **Spectrophotometric Metal Ion Analysis** **Metal Ion for Analysis** --- **A. A Set of Standard Solutions** 1. **Prepare a stock solution.** Show the calculation for the mass of metal ion salt in the preparation of the stock solution. Refer to Prelaboratory Assignment, question 2a. Calculation: \[ 100\text{mL} \times 1\text{L} / 1000\text{mL} \times 0.10\text{mol} / 1\text{L} \times 249.68\text{g} = 2.5\text{g } \text{CuSO}_4\cdot\text{5H}_2\text{O} \] - **Measured tared mass of metal ion salt (g):** 2.499 - **Description of the preparation of the 0.10 M stock solution.** - **Concentration of stock solution (mol/L):** 0.01 M --- **B. Determination of \(λ_{max}\)** 2. **Wavelength Scan.** Use the following table to record the wavelength and absorbance data. | λ | Abs | λ | Abs | λ | Abs | λ | Abs | λ | Abs | |------|-----|------|-----|------|-----|------|-----|------|-----| | | | | | | | | | | | - **Plot the data of absorbance versus wavelength to set \(λ_{max}\). From the data plot, \(λ_{max}\):** 610 nm - **Have the instructor approve your graph.** --- **C. Plot the Calibration Curve** 1. **Absorbance of Standard Solutions.** Read and record the absorbance values for the standard solutions. | Standard Solution | Volume of Standard Solution (μL) | Absorbance | Calculated Molar Concentration | |-------------------|-----------------------------------|------------|--------------------------------| | Blank | 0 | 0.033 | | | 1 | 2 | 0.095 | | | 2 | 5 | 0.763 |
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