B. Metathesis to [Ru(phen)3)]Cl2 The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100 mL dry acetone (add enough to be completely dissolved), if any solids observed filter through medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone and dry in oven at 60-80C. Record yield.
B. Metathesis to [Ru(phen)3)]Cl2 The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100 mL dry acetone (add enough to be completely dissolved), if any solids observed filter through medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone and dry in oven at 60-80C. Record yield.
Chapter16: Applications Of Neutralization Titrations
Section: Chapter Questions
Problem 16.34QAP
Related questions
Question
I need help calculating the theoretical yield of the final product shown in the procedure below!
![B. Metathesis to [Ru(phen)3)]Cl2
The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100
mL dry acetone (add enough to be completely dissolved), if any solids observed filter through
medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with
a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution
to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further
precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone
and dry in oven at 60-80C. Record yield.](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F6fb154a2-fbb2-42ec-8c1b-3d3da9d6adc1%2Fb9430a20-4c56-47c2-aab8-b77a766a7b0e%2F4rli0pr_processed.jpeg&w=3840&q=75)
Transcribed Image Text:B. Metathesis to [Ru(phen)3)]Cl2
The dry [Ru(phen)3] [PF6]2 from Step A is placed in a 250 mL beaker and dissolved in 50 to 100
mL dry acetone (add enough to be completely dissolved), if any solids observed filter through
medium porosity glass frit. Transfer the filtrate to a 250 mL beaker and start gently stirring with
a stir bar. Separately, dissolve 1.25 g Bu4NCI in 25 mL dry acetone. Add the Bu4NCI solution
to the [Ru(phen)3]2+ solution dropwise until it appears that further additions do not induce further
precipitation. Filter product with a 60 mL medium porosity glass frit. Wash with 20 mL acetone
and dry in oven at 60-80C. Record yield.
Expert Solution
This question has been solved!
Explore an expertly crafted, step-by-step solution for a thorough understanding of key concepts.
Step by step
Solved in 2 steps with 3 images
Recommended textbooks for you