4 Pentacarbonyl iron (0), Fe(CO)s, was refluxed for 40h with an equal volume of dicyclopentadiene, C₁0H₁. The volatile material was removed in vacuum, and a crystalline compound was obtained by recrystallization of the residue. The molecular weight was determined by freezing point depression in benzene to be approximately 368 g/mole. Elemental analysis proved the following data: C: 47.55; H: 2.85; Fe: 31.52. The IR spectrum is shown below. Suggest a structure for the compound.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question

O: 18.08

4 Pentacarbonyl iron (0), Fe(CO)5, was refluxed for 40h with an equal volume of
dicyclopentadiene, C₁0H₁ The volatile material was removed in vacuum, and a
crystalline compound was obtained by recrystallization of the residue. The molecular
weight was determined by freezing point depression in benzene to be approximately
368 g/mole. Elemental analysis proved the following data: C: 47.55; H: 2.85; Fe: 31.52.
The IR spectrum is shown below. Suggest a structure for the compound.
4000 3000
Cm-1
1500
2000
1000
800
100
80---
60
40
20+
9
on
8
10
Wavelength, microns
11 12
13
Transcribed Image Text:4 Pentacarbonyl iron (0), Fe(CO)5, was refluxed for 40h with an equal volume of dicyclopentadiene, C₁0H₁ The volatile material was removed in vacuum, and a crystalline compound was obtained by recrystallization of the residue. The molecular weight was determined by freezing point depression in benzene to be approximately 368 g/mole. Elemental analysis proved the following data: C: 47.55; H: 2.85; Fe: 31.52. The IR spectrum is shown below. Suggest a structure for the compound. 4000 3000 Cm-1 1500 2000 1000 800 100 80--- 60 40 20+ 9 on 8 10 Wavelength, microns 11 12 13
Expert Solution
Step 1

Chemistry homework question answer, step 1, image 1

steps

Step by step

Solved in 2 steps with 2 images

Blurred answer
Knowledge Booster
Analytical Separations
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY