Chemistry
Chemistry
10th Edition
ISBN: 9781305957404
Author: Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher: Cengage Learning
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2. Based on the NMR spectrum of the product from part B, did you obtain borneol, isoborneol, or a mixture? Explain. If you obtained a mixture of borneol and isoborneol, what was the percentage of each? Show your calculation below. Which isomer should have predominated (Isoborneol)? Why?Did your results confirm this?
14
NMR
Experiment 6B-product (isoborneol)
10
0.28
20.86
4.016
3.622
FI: 60.011
SWI: 1015
EX: c:left\HIZG.ppg
PW:9.7 us
PD: 3.0 sec
OF1:381.8
NA:4
PTS1d: 8192
LB: 0.0
B. Data/Calculations
Mass of camphor
Mass of isoborneol product
% yield of reaction-part B
calculation: 0.3332
0.2320 g
0.3332 g
143.6
%
× 100%
0.2320
m.p. isoborneol
198-201 °c
PPM
USER: DATE: 03/04/24 (14:16)
DATE:
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Transcribed Image Text:14 NMR Experiment 6B-product (isoborneol) 10 0.28 20.86 4.016 3.622 FI: 60.011 SWI: 1015 EX: c:left\HIZG.ppg PW:9.7 us PD: 3.0 sec OF1:381.8 NA:4 PTS1d: 8192 LB: 0.0 B. Data/Calculations Mass of camphor Mass of isoborneol product % yield of reaction-part B calculation: 0.3332 0.2320 g 0.3332 g 143.6 % × 100% 0.2320 m.p. isoborneol 198-201 °c PPM USER: DATE: 03/04/24 (14:16) DATE:
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