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Cobalt Synthesis Lab Report

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Results and Discussions By using the principle of LeChatlier, one can determine the two Cobalt forms - CoCl4 2- and Co(H2O)6 2+. In order to determine whether or not the solution will shift left or right with respect to equilibrium, it is based on Cl-. However, when silver nitrate was added to bis(tetraethylammonium), it showed that Cl- was reduced in the given solution. This ultimately caused the synthesis of the product turned it a pink color. When given a blue color, it was determined that tetraethylammonium Chloride was involved with the stock solution, which ultimately caused the Cl- to form the reactants. Finally, based from the results, it is shown that CoCl4 2- is blue, and Co(H20)6 2+ is pink. Since we now have determined the two different colors of Cobalt, we can now find constant K. With the help of the spectrophotometer, the absorbance of the stock solutions were measured at 656nm and 519nm respectively. The concentration was determined with the help of Beers Law and the extinction coefficient of each wavelength. Finally, the equilibrium constant was .327x10^-7. CoCl4 2- 6H2O Co(H20)62+ 4Cl- I 0.016 2.8 M 0.00 0.00 C -0.015 -0.09 +0.016 +0.06 E 8.7x10-4 2.6 0.016 0.06 …show more content…

Likewise, the solution was placed in an hot water bath in order for the temperature to rise. Given the solution in the ice bath, it turned pink. Moreover, given the solution in the warm bath, it turned blue. At the wavelengths of 656nm and 519nm, the solutions absorbance’s were recorded at 4degrees Celsius and 40 degrees Celsius. Given the results, one can conclude that the reaction was exothermic. This is true because the reaction shifted to the left when heat was added which ultimately led to the production of more CoCl4

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