Introduction
The objective of this lab will be to proficiently separate a mixture, using filtration and evaporation. In this lab, a homogeneous mixture will be created, along with a heterogeneous mixture.The two mixtures will be mixed together, yet separated. Common substances will be mixed and then separated using two of the techniques already listed; filtration and evaporation.
Theory
If the salt, sand, and water mixture is separated successfully through filtration and evaporation, then the percent recovery of the salt and sand will be 100%.
Salt, sand, and water are each substances that are made up of 2 or more elements chemically combined, or compounds. When mixing compounds, it can be either a homogeneous mixture or a heterogeneous
…show more content…
This will let the filtrate through but leave the sand behind. The filtrate is the liquid that passes through the funnel during filtration. In this experiment, the saltwater solution is the filtrate. The solution remaining in the beaker will then be heated over a Bunsen burner. As the solution is being heated, the water in the saltwater solution will evaporate off until only the salt is remaining in the beaker. Evaporation is a process where a soluble solid is separated from a liquid. The lab ends with the sand on the filter paper, and the salt remaining in the beaker.
In order to successfully reach the objective of the lab, the amount of each substance that is being separated must stay consistent from start to finish. The amount of each substance before it is added to the mixture and after it has been separated needs to be recorded so that comparison and analysis will be correct. All of the data will be used to calculate the percent recovery of the sand and the salt. To find percent recovery, the following equation used will be:
% Recovery = Amount of the substance recovered Original amount of the substance x 100
The answer will then show if separating the mixture was successful, and in turn completing the lab and objective.
Materials
150 mL beaker
Oven
250 mL beaker
Bunsen burner
Stirring rod
Wire gauze
Ring stand
Electronic balance
Iron ring
Sand (SiO2)
Filter paper
Salt (NaCl)
2 spoons
Ceramic fiber square
Funnel
Clay triangle
The purpose of this lab was to determine the limiting reactant in a mixture of to soluble salts and the percent composition of each substance in a salt mixture.
The original 1.0 gram of the 50/50 mixture of the benzoic acid and benzil contain 0.5 gram of benzil. Thus, from 0.5 gram of benzil, only 0.266 gram of benzil was collected. The percent recovery of benzil was calculated to be 53.2%. This low percent recovery could be due to filtration errors. Some amount of benzil remained on the filtration paper that contained the MgSO4. In order for determining the purity of the
Experiment 55 consists of devising a separation and purification scheme for a three component mixture. The overall objective is to isolate in pure form two of the three compounds. This was done using extraction, solubility, crystallization and vacuum filtration. The experiment was carried out two times, both of which were successful.
When we were mixing the filtration and letting it vent periodically, we lost some of it. So our percent recovery is as follows:
Because salt dissolves in water, we added water to the salt and sand mixture. Sand is insoluble in water making the sand not dissolve. The mixture containing of sand and salt water was then filtered with filter paper. The filter paper allowed the salt water to pass through because it is a liquid while not allowing sand to pass through because it is a solid. The salt water was then collected in a pre-weighed 250-mL (67.88 gram) beaker while the sand and filter paper was put in a pre-weighed (52.02 gram) 100-mL beaker. The water was then evaporated because we left both beakers to dry overnight.
The purpose of this experiment is to familiarize oneself with the general procedures determining a partition coefficient at the microscale level and learn in weighing milligram quantities of materials on an electronic balance, the use of automatic pipets, the use of transfer pipet, and the use of a vortex mixer. Also, to familiarize oneself with extraction
The technique I will use to isolate the individual mixes in the blend is paper chromatography.
For the experimental part of this lab, my lab partners and I used six 100 miller liters of beakers and label each baker with concertation percentage of 100%, 50 %, 25 %. 12.5%, 6.25%, and 0%. For the next step of the experiment we used a graduated cylinder
Secondly, the definition of a homogeneous mixture. Homogeneous mixtures are mixtures in which the substance is uniform in structure or composition throughout. Lastly, the definition of heterogeneous mixtures. This is when a solution consists of dissimilar parts of elements or when you can see the individual elements. Our hypothesis was if the properties of individual substances compare with properties of mixed substances and we mix water with cornstarch, then it will create a substance that's properties switch between a solid and liquid that is a homogeneous mixture.
Evaporating is the procedure of a substance in a fluid state changing to a vaporous state because of an increase in temperature or potentially pressure. Evaporation is particularly successful while isolating solvent blends. (Contrasted with filtration, where in spite of the fact that it can at present separate dissolvable blends, its essential and most advantageous utilize is to isolate insoluble blends.) Not at all like filtration, had evaporation fully disposed of the solvent, abandoning no filtrate. Take, for example, a salty water blend. Whenever evaporated, heat is connected, influencing the dissolvable to evaporate, and the solute crystalized. For our assessment the technique of evaporation is done by evaporating the diverse fluids. Juices
The complex mixture of iron fillings, sawdust, sand, oil, water, sugar, salt, red food coloring, and vinegar can be separated using many different separation tactics. First, the iron fillings can be separated using magnetic separation. Second, you would filter out the sand and sawdust. You can mechanically separate the sand and sawdust from each other because they are different enough physically to be able to tell them apart. Next, you would evaporate the liquids, being the water, oil, vinegar, and red food coloring, to leave the salt and sugar behind. You can then mechanically separate sugar and salt because they do not stay together after the other substances evaporate. With the remaining substances you can distill the mixture to separate
This report presents the percentage recoveries found when using the solid-liquid and liquid-liquid extraction techniques to extract a strong acid, weak acid, base, and neutral compound from a mixture. During the solid-liquid section of the experiment, 0.5 M NaHCO , 0.5 M NaOH, 0.5 M HCl, and distilled water are used to dissolve and separate the acid, phenol, and amine solutions from the mixture, leaving the neutral compound remaining. After adding 3 M HCl to the acid and phenol solutions and3 M NaOH to the amine solution, the solutions and solids formed were filtered and the percent recovery of each was calculated. The percent recovery was around a range of 20 % to 22 % for the acid, phenol, and amine, but the neutral had a much higher percentage about 60 %. After using similar techniques for the liquid-liquid extraction section of the experiment, removing the clear lower layer of the two immiscible liquids each time, the percent recovery was around 50 % - 55% for the acid and neutral. The percentages for the phenol and amine were lower. In both sections of the experiment, some percentage of the acid, phenol, amine, and neutral compounds was recovered, so that part of the experiment was successful.
During this experiment students will take a mixture and separate it into its’ pure substances. A mixture is a combination of two or more substance. These substances cannot be combined chemically but more physically. The pure substances are substances that cannot be separated any more by physical means. The students will learn the difference of these two meanings during the experiment.
Knowing specific methods made it possible to separate the substances. This contributed to the purpose of the experiment which was to determine what in the given mixture had the higher percent composition by mass in the sand, salt, and iron mixture. The percent composition is determined by dividing the mass of the mixture by the mass of a substance, and then dividing it by 100. The hypothesis made was that in the given mixture, if the mass of the sand is the greatest, it has the highest percent composition by mass because more of a substance would mean that it has more composition in the mixture.
There are various types of separation techniques for various types of mixtures- sieving, magnetic separation, sublimation, decantation, filtration, centrifugation, evaporation, fractional crystallization, precipitation, fractional distillation, use of separating funnel, chromatography and so on.