Name: Lisa Brewer iLab, Week # 2 CATIONS AND ANION LAB Introduction The purpose of this week’s lab is to learn to demonstrate a double-replacement reaction of ionic compounds. To accomplish this, two ionic compounds will be mixed together and the product will precipitate out of solution. In this procedure, the product must be precipitated out of the solution and then weighed. For this lab, lead (II) nitrate (Pb(NO3)2) and potassium chromate (K2CrO4) will be reacted together to demonstrate double replacement reaction between 2 ionic compounds. This was shown when chromate replaced the nitrate and formed lead (II) chromate, and when the nitrate replaced the chromate and formed potassium nitrate, which is shown in the …show more content…
This indicates a reaction occurred and precipitate has formed and settled on the bottom of the beaker. Set up the Erlenmeyer flask with a Buchner funnel. Select equipment from toolbar, then from the dropdown menu, select Erlenmeyer flask—250mL. Right click the Erlenmeyer flask, choose Buchner funnel. The Buchner funnel will be added to your Erlenmeyer flask. Select the 100mL beaker and right click on Pour/Decant. The flask will turn on its side so that you can move the beaker above the Buchner funnel. The solution will pour into the funnel when positioned correctly. Note: When the solution has been filtered, a white area will appear on the bottom of the flask. Right click the flask. Select Buchner funnel. Message window appears with question. Select place solid into 50mL Test tube. Click OK. Note: a test tube will appear with a small amount of precipitate on the bottom. To measure the weight of the precipitate, right click the test tube. Select show weight. The weight of the precipitate will appear below the test tube. Record this information in the Observations and Results section of the lab report, including the weight and appearance of the precipitate. Observations and Results The appearance of the precipitate was shown several ways during the experiment. In the 100mL beaker, after both chemicals were added, it was shown as a dotted solution. It was then shown as a solid and a white color in
Next clamp the vacuum flask securely to a clamp and stand, attaching the Buchner funnel to the top with the use of a rubber funnel
Introduction – A double replacement reaction is a chemical reaction between two compounds where the positive ion of one compound is exchanged with the positive ion of another compound. If you have the reactants of two reaction solution that you can determine the products. All you need to do is pair the positive parts of the compounds with the other compounds negative part. Once you find the products you can determine their phase of matter by using Table H. You can also use Table F to determine the solubility guidelines for aqueous solutions. If the product falls under soluble or exceptions to insoluble it is in the aqueous stare. If the product falls under
To study the nature of ionic reactions, write balanced equations, and write net ionic equations for precipitation reactions.
B1. Work under the hood! Weigh out exactly 0.1 g of ammonium dichromate and add to a test tube. Clamp and warm gently with a Bunsen burner. Two of the products of this reaction are chromium(III)oxide and nitrogen gas. Watch for evidence of the third product.
Next, I poured distilled water just below the 250ml mark on the neck of the volumetric flask.
c) Record the amount of substance that dissolved – all, some, a little, or none.
solutions using qualitative analysis techniques. 1 Silver (Ag + ) and lead (Pb 2+ ) created a solution of
The purpose of this experiment is to study ionic reactions, to be able to write balanced equations, and to be able to write net ionic equations for precipitation reactions.
Every reaction that occurred during this lab was a double replacement reaction, or a chemical reaction in which two aqueous compounds react with each other and result in two different compounds where one is either a solid precipitate, a liquid (water), or a gas. A precipitate in this case is a solid that exits the aqueous solution during the chemical reaction because it is too heavy to stay in the solution. Clear signs of a chemical reaction occurring is the formation of a precipitate, especially in a double replacement reaction, as well as the release of gas bubbles and the product of an acid. During a double replacement, the elements “switch partners” as seen with the base equation for all double replacement reactions, AB+CD→AC+BD. For a lab such as this, a hand lens could be used to confirm the presence of gas bubbles or a precipitate that would not have easily been seen without the device.
When filling up the burette it is important that a funnel is used, however as the solution reaches the 0 mark it is ideal that the funnel be removed and a pipette used instead to reach the 0 mark, this is to achieve greater precision. During the experiment, it is important to swirl the flask continuously with one hand
Dispense .5 mL water into the already weighed conical vial, replace cap and face insert on its down side.
Place a burette on the conical flask and then hold it by using a clamp stand.
5. Wet the paper with distilled water to hold it in place in the funnel. Transfer all the solution and the precipitate from the beaker using a rubber policeman. Wash the precipitate with two or three 5-mL portions of distilled water. Do this by adding each portion to the beaker in which you did the precipitation to transfer any remaining
At the end of the experiment when the lid was removed, it was found out that the blue colour of the copper (II) sulphate solution has faded away. It was turned to pale grey and there were some precipitates present. It was the zinc powder that was in excess to ensure that the copper (II) sulphate solution could react fully with the zinc powder.
Heavy precipitate emerged immediately and solution turned white in color; solution then became opaque and turned light, bright blue in color.