How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove

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An oxidation reaction was conducted using cyclohexanol and NaOCl to make cyclohexanone. How can we know that the NMR for cyclohexanone is in fact cyclohexanone( the NMR for cyclohexanone is not labeled). Analyze the spectra to prove its identity along with the NMR of the starting material which is the spectra labeled cyclohexanol below.

471
BRUKER
I222
|TV ||
Current Data Paramet ers
Feb20-2020-chem22:
67
NAME
EXPNO
PROCNO
1
Cyclohexanol in CDC13
F2 - Acquisition Parameter
Date
Time
20200220
23.13
INSTRUM
PROBHD
spect
5 mm PABBO вв-
zg30
32768
PULPROG
TD
SOLVENT
NS
CDC13
2
DS
SWH
5208.333 Hz
0.158946 Hz
3.1457281 sec
16
96.000 usec
25.61 usec
298.0 K
FIDRES
AQ
RG
DW
DE
ТЕ
D1
1.50000000 sec
TDO
1
------- CHANNEL f1
NUC1
P1
-- -
-
1H
11.38 usec
-2.50 dB
18.35869598 w
PL1
PL1W
SFO1
400.1320007 MH2
F2 - Processing parameters
SI
SF
32768
400.1300065 MHz
WDW
SSB
EM
0.30 Hz
LB
GB
PC
1.00
7.5
7.0
6.5
6.0
5.5
5.0
4.5
4.0
3.5
3.0
2.5
2.0
1.5
1.0
ppm
888
Transcribed Image Text:471 BRUKER I222 |TV || Current Data Paramet ers Feb20-2020-chem22: 67 NAME EXPNO PROCNO 1 Cyclohexanol in CDC13 F2 - Acquisition Parameter Date Time 20200220 23.13 INSTRUM PROBHD spect 5 mm PABBO вв- zg30 32768 PULPROG TD SOLVENT NS CDC13 2 DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 16 96.000 usec 25.61 usec 298.0 K FIDRES AQ RG DW DE ТЕ D1 1.50000000 sec TDO 1 ------- CHANNEL f1 NUC1 P1 -- - - 1H 11.38 usec -2.50 dB 18.35869598 w PL1 PL1W SFO1 400.1320007 MH2 F2 - Processing parameters SI SF 32768 400.1300065 MHz WDW SSB EM 0.30 Hz LB GB PC 1.00 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 ppm 888
3
...
BRUKER
Current Data Paramet ers
NAME
EXPNO
Feb18-2020-chem22:
3
PROCNO
1
F2 - Acquisition Paramet er
Date_
Time
INSTRUM
PROBHD
20200218
17.31
spect
5 mm PABBO BB-
zg30
32768
CDC13
2
1.8 1.7
1.6 ppm
PULPROG
TD
SOLVENT
2.9
2.8
2.7
2.6
2.5
2.4 2.3
2.2
2.1
2.0
1.9
NS
DS
SWH
5208.333 Hz
0.158946 Hz
3.1457281 sec
64
96.000 usec
FIDRES
AQ
RG
DW
DE
25.61 usec
298.0 K
1.50000000 sec
1
TE
D1
TDO
CHANNEL f1 =--
1H
11.38 usec
-2.50 dB
18.35869598 W
400.1320007 MH2
===== =-
NUC1
P1
PL1
PL1W
SFO1
F2 - Processing parameterS
32768
400.1300065 MHz
SI
SF
WDW
EM
SB
LB
0.30 Hz
GB
PC
1.00
11
10
8
7
6
5
4
3
2
1
ppm
000'
2.32
1.044
-2.08
88:I
98:T/
1.85
1.70
1.70
69'I
89
Transcribed Image Text:3 ... BRUKER Current Data Paramet ers NAME EXPNO Feb18-2020-chem22: 3 PROCNO 1 F2 - Acquisition Paramet er Date_ Time INSTRUM PROBHD 20200218 17.31 spect 5 mm PABBO BB- zg30 32768 CDC13 2 1.8 1.7 1.6 ppm PULPROG TD SOLVENT 2.9 2.8 2.7 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 NS DS SWH 5208.333 Hz 0.158946 Hz 3.1457281 sec 64 96.000 usec FIDRES AQ RG DW DE 25.61 usec 298.0 K 1.50000000 sec 1 TE D1 TDO CHANNEL f1 =-- 1H 11.38 usec -2.50 dB 18.35869598 W 400.1320007 MH2 ===== =- NUC1 P1 PL1 PL1W SFO1 F2 - Processing parameterS 32768 400.1300065 MHz SI SF WDW EM SB LB 0.30 Hz GB PC 1.00 11 10 8 7 6 5 4 3 2 1 ppm 000' 2.32 1.044 -2.08 88:I 98:T/ 1.85 1.70 1.70 69'I 89
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