Which of the following is incorrect: a. General steps in quantitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Qualitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a direct proportionality between a measured property and the concentration or amount of substance. Please fill in the spaces one of the following characters (a or b or c or d or e)

Which of the following is incorrect: a. General steps in quantitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Qualitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a direct proportionality between a measured property and the concentration or amount of substance. Please fill in the spaces one of the following characters (a or b or c or d or e)

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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Which of the following is incorrect: a. General steps in quantitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Quantitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a inverse proportionality between a measured property and the concentration or amount of substance. Please fill in the spaces one of the following characters (a or b or c or d or e) Answer:
Which of the following is incorrect: a. General steps in quantitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Quantitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a inverse proportionality between a measured property and the concentration or amount of substance.
analytical balanceb. top-loading balancec. serological pipetted. graduated cylindere. burettef. volumetric flaskg. Erlenmeyer flaskh. beaker Define the term, “measurement uncertainty”. Among the instruments listed above, which ones have the highest uncertainty? Which ones have the lowest?
1. Samples that should not be stored should be prepared/analyzed as soon as possible, especially for measurement…a. hardnessb. Nitritec. Conductivityd. Phenol 2. The following are general sample treatments in pesticide analysis, except…a. Extractionb. Cleaningc. Concentrationd. Filtering
(8) Identify whether the following are examples of systematic or random error or are mistakes: a. Using an inaccurately calibrated buret. b. An uncertainty of 1 mg in the weight of your sample.∓ c. Overshooting the endpoint on your first sample, then hitting the endpoint on the remaining samples.d. Failing to let your volumetric pipet drain for a few seconds have most of the liquid has been delivered.
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The method described above is to be used for the analysis of ores that assay about 1.2% gold. What minimum sample mass should be taken if the relative error resulting from a 0.4-mg loss is not to exceed a. -0.1% b. -0.8%
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2. What measurements might you record regarding water samples to assist with the quantification process? How might these measurements have error introduced? 3. Create a table of your observations made during the experiment. For example: Sample 2 Sample 1 Initial After shaking Write a brief summary of any conclusion that were reached. 4. With your group, write a sentence statement of the objective of the experiment and the method that will be used.
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28 Report Sheet Separation of the Components of a Mixture D. Determination of Percent Recovery Mass of original sample 10.588 Mass of determined (NH Cl+ NaCl+ SiO2) 1-88 8 Differences in these weights g matter recovered Percent recovery of matter %3D = %00 % g original sample Account for your errors. Combor QUESTIONS 1. Could the separation in this experiment have been done in a different order? For example, if the mixture was first extracted with water and then both the extract and the insoluble residue were heated to dryness, could you determine the amounts of NaCl, NH,Cl, and SiO, originally present? Why or why not? Consult a handbook to answer these questions. 2. How could you separate barium sulfate, BaSO4, from NaCl? 3. How could you separate magnesium chloride, MgCl2, from silver chloride, AgCl? 4. How could you separate tellurium dioxide, TeO2, from SiO,? 5. How could you separate lauric acid from a-naphthol? (See Table 3.1.)