The test tube used in the determination of the AHrxn for nitric acid was still wet with water. [ magnitude of AHrxn] The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated value. [Ccal The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated value. However, the NaOH solution used in the determination of AHrxn was of the correct concentration. [magnitude of AHrxn] A wet pipette was used to transfer 10.00 mL of 1M HNO3 in the determination of AHrxn. [magnitude of AHxn) The thermometer and stopper were inserted to the test tube 5 minutes after adding the base in the calibration part. [Ccal]

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter27: Molecular Fluorescence Spectroscopy
Section: Chapter Questions
Problem 27.9QAP
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Calorimetry - Heat of Neutralization

Cause and Effect: Identify the effect of the condition on the indicated parameter. Write increase, decrease, or no effect, and provide an explanation.

Calibration part: HCl and NaOH (limiting reagent)

Determination of enthalpy change part: HNO3 and NaOH (limiting reagent)

The test tube used in the determination of the AHrxn for nitric acid was still wet with water. [ magnitude of AHrxn]
The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated
value. [Ccal
The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated
value. However, the NaOH solution used in the determination of AHrxn was of the correct concentration. [magnitude of
AHrxn)
A wet pipette was used to transfer 10.00 mL of 1M HNO3 in the determination of AHrxn. [magnitude of AHxn]
The thermometer and stopper were inserted to the test tube 5 minutes after adding the base in the calibration part. [Ccal
Transcribed Image Text:The test tube used in the determination of the AHrxn for nitric acid was still wet with water. [ magnitude of AHrxn] The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated value. [Ccal The actual concentration of the sodium hydroxide used in the calibration part of the experiment was lower than the stated value. However, the NaOH solution used in the determination of AHrxn was of the correct concentration. [magnitude of AHrxn) A wet pipette was used to transfer 10.00 mL of 1M HNO3 in the determination of AHrxn. [magnitude of AHxn] The thermometer and stopper were inserted to the test tube 5 minutes after adding the base in the calibration part. [Ccal
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