In the attached H1-NMR, draw and identify each set of equivalent hydrogens in the structure and list peak they belong to in the NMR spectrum. 87.241H NMR of Product from Week 2Dihydrosafrole SynthesisF1: 60.201EX: c:\eft\H1\ACQ.ppg6.8146.7367699 96.524CH 35.9925.9255.8969SW1: 3994PW: 2.4 us5PD: 3.5 secOF1: 361.3NA: 53.1912.6142.5042.3733LB: 0.01.8491.7571.6641.5521.5221.4541.4082PTS1d: 40961.2801.0130.9490.8930.8410.7850.7280.000PPMUSER: -- DATE: 02/21/24 (15:18)0

NMR spectrum is an analytical technique that can be used to identify the hydrogen (H) atoms present…

Answered: In the attached H1-NMR, draw and…

In the attached H1-NMR, draw and identify each set of equivalent hydrogens in the structure and list peak they belong to in the NMR spectrum.

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter45: Synthesis And Bioassay Of Sulfanilamide And Derivatives

Section: Chapter Questions

Problem 5Q

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Concept explainers

Mass Spectrometry

This process is an instrumental method in which a sample is changed to fast moving positive ions by electron bombardment. The charged particles vary due to their different mass to charge ratio and are estimated with the help of this difference. It is also called mass spectroscopy.

Question

In the attached H1-NMR, draw and identify each set of equivalent hydrogens in the structure and list peak they belong to in the NMR spectrum.

8
7.241
H NMR of Product from Week 2
Dihydrosafrole Synthesis
F1: 60.201
EX: c:\eft\H1\ACQ.ppg
6.814
6.736
7
699 9
6.524
CH 3
5.992
5.925
5.896
9
SW1: 3994
PW: 2.4 us
5
PD: 3.5 sec
OF1: 361.3
NA: 5
3.191
2.614
2.504
2.373
3
LB: 0.0
1.849
1.757
1.664
1.552
1.522
1.454
1.408
2
PTS1d: 4096
1.280
1.013
0.949
0.893
0.841
0.785
0.728
0.000
PPM
USER: -- DATE: 02/21/24 (15:18)
0

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