Answered: First paragraph: Discuss what is meant…

First paragraph: Discuss what is meant by a titration. Discuss the terminology used in a titration. Ex. endpoint, equivalence point, primary standard, secondary standard, indicator.

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter17: Complexation And Precipitation Reactions And Titrations

Section: Chapter Questions

Problem 17.16QAP

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The equation for a reaction by which a solution of sodium carbonate may be standardized is 2HC7H5O2+Na2CO32NaC7H5O2+H2O+CO2. A student determines that 5.038g of HC7H5O2 uses 51.89mL of sodium carbonate solution in the titration. Find the molarity of the sodium carbonate.
1. Calcium in a sample solution is determined by atomic absorption spectroscopy (AAS). A stock solution of calcium is prepared by dissolving 1.834 g CaCl, 2H,0 in water and diluting to 1 litre. From this stock solution, the second stock solution is prepared by the dilution factor of 10. Three standard solutions of calcium are prepared from the second stock solution with the following dilution factor: 20 (first standard solution), 10 (second standard solution) and 5 (third standard solution). A blank solution is prepared as well. Absorbance signals of AAS are as follows: 1.5 (blank solution), 10.6 (first standard solution), 20.1 (second standard solution), 38.5 (third standard solution), 29.6 (sample solution). (Molar mass; Ca = 40.00 g mol-, CI = 35.45 g mol-, 0 = 16.00 g mol-', H = 1.00 g mol-1) a. Construct ONE (1) plot that could be used to represent the calibration curve. b. From the plot of Q1a, determine the amount of calcium in parts per million.
(1) Careless Carlie weighed her KHP sample, but forgot to bring her report sheet along, so she recorded the mass of KHP on a paper towel. During her titration, which required 18.46 mL of base, she spilled some base on her hands. She remembered to wash her hands, but forgot about the data on the towel, and used it to dry her hands. When she went to calculate the molarity of the base, Carlie discovered that she didn’t have the mass of her KHP. Her kindhearted instructor told Carlie that her base was 0.2987 M. Calculate the mass of Carlie’s KHP sample. Show calculations (2) What mass of solid NaOH would be needed to make 645 mL of Carlie’s NaOH solution? Show calculations.
Average the two percentages and calculate the percentage difference. given : Concentration of acetic acid in the 100 mL sample of titration 1 = 3.238 % Concentration of acetic acid in the 100 mL sample of titration 2 = 3.099 % NaOH vs CH3COOH Burette solution is NaOH and the pipette solution is 5.0 mL of Vinegar Titration Initial burette reading Final burette reading Volume of NaOH consumed Average volume of NaOH Approximate 0.0 mL 20.1 mL 20.1 mL 20.3 mL Titration 1 0.0 mL 20.9 mL 20.9 mL Titration 2 0.0 mL 20.0 mL 20.0 mL To find the average volume Average volume = 20.1 mL + 20.9 mL + 20.0 mL320.1 mL + 20.9 mL + 20.0 mL3 = 20.3 mL Concentration of Vinegar = Volume of NaOH * Concentration of NaOHVolume of vinegarVolume of NaOH * Concentration of NaOHVolume of vinegar = 20.3 mL * 0.0647 M5.0 mL20.3 mL * 0.0647 M5.0 mL = 0.2627 M Concentration of NaOH = Volume of…
Details Preparation of Dilute Table Solution Molarity of I₂ Standard Solution Molar Mass (g/mole) Ascorbic Acid Number of Tablets per Analysis Mass (g) Container plus 1 Tablet Mass (g) Container less 1 Tablet Mass (g) of 1 Tablet Volume (mL) of Dilute Tablet Solution Titrimetric Analysis of Dilute Tablet Solution Volume (mL) of Aliquot Portion of Dilute Tablet Solution Titrated Final Buret Reading (mL) Initial Buret Reading (mL) Volume (mL) I₂ Solution Delivered No. of mmol 1₂ Reacted No. of mmol Ascorbic Acid in Aliquot Total No. of mmol Ascorbic Acid Present in the Volumetric Flask Total Mass (mg) of Ascorbic Acid Present in 1 Tablet Average Mass Ascorbic Acid/Tablet Deviation Standard Deviation Coefficient of Variation (%RSD) Reported Composition of Tablet Trial 1 50.00 11.64 0.20 0.02512 M 176.14 1 12.2546 11.7824 0.4722 250.00 Trial 2 50.00 22.80 11.64 Trial 3 250 mg Ascorbic Acid/Tablet 50.00 11.20 0.00 mg Ascorbic Acid/Tablet
Part 1: Preparation of the Primary Citric Acid Standard 1. Mass of Citric Acid: 4.05 g 2. Volume of Citric Acid Solution: 0.75 ml (at the equivalence point) 3. Moles of Citric Acid: (Molar Mass = 192.0 g/mol) 4. Molarity of Citric Acid Solution: Part 2: Titration of the Sodium Hydroxide Solution (Show your work on page 4) 1. Volume of Citric Acid at the Equivalence Point 2. Moles of Citric Acid at the Equivalence Point: 3. Moles of NaOH at the Equivalence Point 3 NaOH + H.CaHsO, → Na:CH.O, + 3 H,O 4. Volume of NaOH 10.0 mL 5. Calculated Molarity of NaOH: Do not use the dilution equation to calculate the molarity of the sodium hydroxide. The dilution equation cannot be used when a reaction is occurring
Titration of Vinegar Experimental Data Trial 1 Trial 2 Initial Buret Reading 0.05 mL 0.02 mL Final Buret Reading 25.25 mL 23.22 mL Volume of base used Molarity of base used 0.1045 M 0.1045 M Volume of vinegar used 5.00 mL 5.00 mL
For the CO2 impact experiment station: 1) Obtain two plastic cups, red cabbage indicator, a straw, and plastic wrap. 2) Fill each cup approximately one-quarter to one-third full of tap water and add ~10 mL of the red cabbage indicator. 3) Place the two cups side by side on a sheet of white paper. 4) Place the straw into one of the beakers and cover that beaker with the plastic wrap. 5) Carefully blow bubbles into the test cup for 3 min. and observe both cups. 6) Compare the color to the control cup and record any differences. This the Question: Did the beaker with the solution into which CO2 was bubbled change pH/color? By how much? Is this what, you would predict, based on your knowledge of the chemistry of CO2?
Part A) A 10.0 mL sample of 0.250 mol/L NiF2(aq) is mixed with 20.0 mL of 0.0900 mol/L NaOH(aq) and then diluted to a final volume of 100. mL.Calculate the concentration of Ni2+ ions in the 100 mL mixture before the reaction starts. Express your answer to three significant figures.ksp: 5.48e-16
K2CO3 (aq)+ CaCl2 (aq)→ CaCO3 (s) + 2KCl (aq) Data Sheet Table 1: Data and Observations Material Mass CaCl2 2.0g K2CO3 2.5g Filter Paper 1.6g Watch Glass 35.8g Filter Paper + Watch Glass + Precipitate 38.9 Precipitate 1.5g Table 2: Mass of CaCl2 after 24 Hours Initial Observations 24 hour Observation Weigh Boat Mass of Weigh Boat 0.5g Mass of Weigh Boat 0.5g CaCl2 2.0g Mass of CaCl2 2.4g Mass of CaCl2 Calculate the theoretical yield of the solid precipitate. Then use that to calculate the percent yield of the solid precipitate.
A (aq) + ...B(aq) C(s) + D (aq) ... .. Experimental | Volume of B/ mL Mass of Run precipitate/g 1 1.2 5.40 2 1.4 7.24 1.6 9.02 4 1.8 9.90 2.0 10.86 6. 2.2 10.90 7 2.4 10.88 8 2.6 10.84 9. 2.8 10.86 A series of experiment was performed to determine the mole ratio of a given reaction. 1 mL of 1 Molar A added to nine beakers, then the increasing amount of 1 Molar B added to these beakers. Volume of B and mass of precipitate of C are given in the table below. Find the mole ratios through plotting a graph.
3.) In the assay of NaHCO3, 3.0g of the solid is dissolved in 25mL water. What is the normality? How many mL of 1N H2SO4 will be required to neutralize this solution? From this volume of acid, compute the percent purity of NaHCO3.