Finding Molecular Weights from Experimental Data a. Endgroup analysis by titration: 9.8 mols of 1,6-hexanediamine were reacted with 9.8 mols of adipic acid. After the reaction, a titration was performed using KOH. If exactly 65 mL of 5 M KOH were used to neutralize the residual -COOH groups, what is the number average molecular weight of the polymer?
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- Explain a method for titration of HNO3-H2SO4 mixtures ?The Merck Index indicates that 10 mg of guanidine,CH5N3, may be administered for each kilogram of bodymass in the treatment of myasthenia gravis. The nitrogenin a 4-tablet sample that had a total mass of 7.50 g wasconverted to ammonia by a Kjeldahl digestion, followedby distillation into 100.0 mL of 0.1750 M HCl. Theanalysis was completed by titrating the excess acid with11.37 mL of 0.1080 M NaOH. How many of thesetablets represent a proper dose for a patient who weighs(a) 100 lb, (b) 150 lb, and (c) 275 lb?A sample may contain NaOH, NazCO3 and NaHCO3, alone or in some combination, along with inert material. A samplewitha mass of 857.6 mgwas dissolved and titrated with0.1163 M HCI. The volume of HCl used from 0 to methyl red endpoint (Phenolphthalein endpoint was not monitored here) was found to be 36.54 mL. Another 228.8 mg portion of the sample was titrated to the phenolphthalein endpoint and 10.82 mL was used up for this titration. a. What is the composition of the sample? b. Calculate the percentage of each of the component present.
- A student dissolved 3.72 g of sodium p-nitrobenzoate (MW 189.10 g/mol) in 20 mL H20. The solution was then acidified to a pH of 1 using 10% HCI after which a crystalline precipitate of p-nitrobenzoic acid was obtained. The reaction is given below: H-CI O. HO, Nat sodium p-nitrobenzoate p-nitrobenzoie acid The p-nitrobenzoic acid (MW 167.12 g/mol) was collected by vacuum fitration and was found to weigh 2.60 g. Determine the percent yield for this reaction. Provide your answer to 3 significant figures.A 10.00mL sample of alcoholic ethyl acetate was diluted to 100.00 mL. 20.00 mL was aliquoted and mixed with 40.00 mL of 0.04672 M KOH. The resulting mixture was heated for 2 hours. CH3COOC2H5 + OH- → CH3COO- + C2H5OH After cooling, the excess OH was back titrated with 3.41 mL of 0.05042 M H2SO4. Answer the following: Calculate the number of moles of OH- that reacted with ethyl acetate. Calculate the number of moles of ethyl acetate in the 20.00 mL solution. What is the mass of ethyl acetate (FW=88.11 g/mol) in the original 10.00 mL sample?Many chemical reactions are carried out in the presence of buffers. Use the Henderson-Hasselbalch equation to provide a recommendation for a suitable acete/acetic acid buffer under the following reaction conditions. a) If a checial reaction produces hydroxide ion, H3O+, what would be the range for the target pH of a buffer soution that would favor pH stabilizatoin under these conditions? Explain.
- In a titration of methylamine CH3NH2 (pKb = 3.34) with HNO3, which of the following color indicator is preferred? You may refer to the lecture slides to find their transition range. Erythrosin B Alizarin m-Nitrophenol Bromthymol blue Phenol Red0.641 g of a semi-synthetic alkaloid was dissolved in 25 ml of 1% w/v acetic acid and wasanalysed directly by HPLC. The solution was found to contain 1.42 mg/100 ml of an impurity.What is the level of impurity in % w/w and ppm? Calculate the pH of a buffer system made by dissolving 1.2 g of acetic acid and 0.82 g ofsodium acetate in 500 ml of distilled water (pKa of acetic acid = 4.7)A 300mg sample containing Na2CO3, NaHCO3 and NaOH and inert material either alone or in some combination was dissolved and titrated with 0.1M HCl. The titration required 24.41 mL to reach the phenolphthalein endpoint. And an additional 8.67mL to reach the methyl red end point. Determine the composition of the sample and calculate the percent of each titrated component.
- How many grams of dipotassium succinate trihydrate (K2C4H4O4-3H,O, MW = 248.32 g/mol) must be added to 610.0 mL of a 0.0587 M succinic acid solution to produce a pH of 5.835? Succinic acid has pKa values of 4.207 (pKal) and 5.636 (pK42). mass: gHEPES ((4-(2-hydroxyethyl)-1-piperazine ethane sulfonic acid) is a commonly used cell culture buffer with a pKa of 7.5. If you need to prepare 500 mL of 0.2 M HEPES, pH 6.9, how much would you need of the following stock chemicals: 1.0 M HEPES, pH 8.0; 6 M HCI; 6 M NaOH; and distilled H2O?Claire needs to determine the identity of a hydroxide precipitate in an unknown analysis. An HCl titrant required 98 mL to reach the methyl orange endpoint with 0.5401 g of NaCO3 (99.95 %) dissolved in 50 mL freshly boiled distilled water. She then mixed the precipitate in 25 mL of water then filtered out any remaining solids. Titration of the solution required 51.8 mL of standard HCl titrant to reach the phenolphthalein endpoint. What is the concentration of the HCl titrant (M)? What is the concentration of [OH-] (M)?