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(31) Which of the following structures corresponds to the attached 1H-NMR spectrum?
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- For C NMR calculate the chemical shift in ppm for signals 1-7For the following 9 compounds (most of which were the ones used in this lab), tell me what peaks you would expect to see in the 'H-NMR spectrum of those compounds. I have provided table for you to fill out with approximate chemical shift (ppm units), peak multiplicity_(singlet, doublet, etc.) and integration of the signal (how many protons would give that signal). No IR data is required. In addition, tell me the number of 13C-NMR signals you would expect to see [specific 13C shifts are not required] Predict13C NMR Analysis of Aspirin Chemical Shift (Observed ppm) Assignment(s) (A'-J') Expected Chemical Shift Range (ppm) B' D' E' JOH Acetylsalicylic Acid (Aspirin) 169 & 170 152 125 135 (4 peaks) - 122 20 160 140 120 100 Figure 14.13 125.7-MHz 13C-NMR spectrum of aspirin in CDCl3. solvent 80 60 40 20 ppm
- Typo: The chemical formula is missing an oxygen. It should read as: C10H1202. Choose the correct structure of the compound with the following data. Formula: C10H120 100 - 50 4000 3000 2000 1500 1000 500 Wavenumber (3) (2) (5) múltiplet (2) 9 8 6 4 PPM II Ph - C-о-сH,CH-CH3 || Ph-c-CH2 -0-CH2CH3 || Ph -C- CH2CH2-0- CH3 A) B) Structure A O Structure B Structure C O=U O=U O=U TransmittanceQu X Studen M Inbox Wordle | E Intro A Home Forest + data co E Project | Meetin Title + OASIS & Shared + O is.edu/courses/848465/quizzes/234535/take Question 17 Br A B OH ملا تو E OH C 6 pts G H D H F How many different signals would you expect to see in the 1H NMR of the given compounds? (i.e. different chemical shifts)? Compound A = Compound B = Compound C = Compound D = Compound E = Compound F = Search 10:28 PM 3/15/2024 4What effect does increasing the operating frequency of a 1H NMRspectrum have on each value: (a) the chemical shift in 5; (b) thefrequency of an absorption in Hz; (c) the magnitude of a couplingconstant J in Hz?
- A4 The chemical shift of signed proton H at 500MHz was 5ppm. Show the coupling pattern using graphical analysis. And what Hz is the frequency? When measured in 300MHZ, what is the change in frequency and couping constant? Explain.Interpret 1HNMR peaks of ethyl acetate include structureIdentify the following in the given IR Mass spectrum. Compound 1 Mass Spectroscopy: Interpretation of peaks: Compound 1 Mass Spectroscopy: MASS SPECTRUM 100 80 60 40 20 0.0- 10 20 30 40 50 60 70 m/z Interpretation of peaks: Rel. Intensity
- /351142db-11b4-465e-8145-7af70e490f5f/jsf/delivery/deliverAsSsessment Soru 4/8 15 Puan Analyse the high resolution proton NMR spectrum and suggest a compound and write its name. Aslo write down which parts of the molecule belongs to each peak. wg er 's 00 H Spectum C,H1002 Expanded peak duster at 2 32 ppm Expanded peak ster at413 pom Expanded peak clusters at 1 26 and 114 ppm (Maksimum karakter sayısı: 60000) << Zengin-Metin Editorunu (ye karakter hesaplamal Goster Tumüno goster 101 A Organicstructuresf..pdf TR 11.02 2021Attached is the 13C-NMR Spectrum of 1,2,3,4-tetraphenylnapthalene (CDCl3) Can you provide (chemical shift (experimental),chemical shift (literature), assignment) Chemical shift δ(ppm) Experimental Chemical shift δ(ppm) Literature Assignment7.) From the following sets of data, please propose a reasonable structure for the unknown organic compound. This molecule is entirely composed of C, H, and N only. Please show all of your work and feel free to write on the spectra any clues as to the structure. 4000 3000 2000 1000 S DO Infrared spectrum of unknown. KBr salt plate sample. 100 MS-NU-6396 80 60 40 20 - 10 20 30 40 50 60 70 80 90 100 110 m/z Mass spectrum of unknown. Molecular ion = 83.1 Relative Intensity